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E <br /> ANALYTICAL <br /> BSKLABORATORIES <br /> �I . <br /> c ' <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 03/14/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission #: 2002021116 <br /> BSK Sample ID#: 185088 <br /> Project ID: DISCO Project Desc: 1st QTR 2002 GW <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 02/21/2002 <br /> I Sample Description: MW-2 Time Sampled: 1338 <br /> Sample Comments; Date Received: 02/24/2002 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 250 }tg/L 50 1 50 03/05/2002 03/05/2002 <br /> Benzene EPA 8020 Q.81 µg/L 0.3 1 0.3 03/05/2002 03/05/2002 <br /> Ethylbenzene EPA 8020 5.4 µg/L 0.3 1 0.3 03/05/200203/05/2002 <br /> Toluene EPA 8020 0.64 µg/L 0.3 1 0.3 03/05/2002 03/05/2002 <br /> Total Xylenes EPA 8020 14 µg/L 0.3 1 0.3 03/05/2002 03/05/2002 <br /> 1,2-Dibromoethane EPA 8260 ND µg/f, 5.0 1 5 03/05/2002 03/05/2002 <br /> 1,2-Dichloroethane EPA 8260 ND µg/L 5.0 1 5.0 03/05/2002 03/05/2002 <br /> tert-Butyl Alcohol EPA 8260 ND gg/L 50 1 50 03/05/2002 03/05/2002 <br /> Surrogate <br /> Fluorobenzene EPA 8020 92,7 %Rec - 1 NIA 03/05/2002 03/05/2002 <br /> Toluene-d8 EPA 8260 100.5 %Rec - 1 N/A 03/05/2002 03/05/2002 <br /> r <br /> I <br /> i mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H: Analyzed outside of hold time <br /> mg/Kg:Milligrams/Kilogram(ppm) DLR: Detection Limit for Reporting P: Preliminary result <br /> 4g/L.Micrograms/Liter(ppb) :PQL x Dilution S:Suspect result. See Cover Letter for comments. <br /> 1ag/Kg:Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec:Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: 11111111111111111!III!!Il11111111111111111111111111111]1111111111111111111111111 IN Page 2 of 8 <br /> 1. 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />