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v ::�4;tlJC �i�:�°�'f-•;Y:: �i�=�:a'.s��si::�e'.�z :ci'.�e:�: g •il• I • �iii e••• '• •. REPORT COMMENTS 1) ALL pages of this raport are integral parts of the analytical data. Therefore, this report should be reproduced only in Its entirety. 2) soil, sediment oro sludge sample results are reported on a "dry weight" basis except when analyzed for Landfill disposal or incineration parameters. All other solid metriX vamplea are reported on an "as received" basin unlers noted differently, i 3) Reporting Limits are adjusted for sample site used, dilutions and moisture content if applicable. 4) The test results for the noted analytical method(o) meet the requirements of NELAC. Lab Cert. ID# 100201 5) Arilana Envirohmental Laboratory License number AZ0643. 6) According to 40CFR Part 136.3, pH, Chloride Residual and Dissolved Oxygen analyses are to be performed Im"ediately after aqueous sample collection. When these parameters are not indicated as field (e.g. pH Field) they were not analyzed immediately, but ae goon as possible on laboratory receipt. Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) Inorganic Qualifiers (Q-Colum) U AnaLyte was not detected at or above the reporting limit. -f Not detected at or above the reporting limit. J Result is less than the RL, but greater than or equal to the method detection Limit. 8 Result Is less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F WEE: Result is less than the RL, but greater than or equal to the method detection Limit_ Inorganic Flags (FLag Column) ICY,CCV,ICS,CCB,ISA,ISB,CRI,CRA,MRL: Instrument related QC exceed the upper or lower control limits. " LCS, LCU, NO: Batch QC exceeds the upper or lower control Limits. j + MSA correlation coefficient is less than 0.995. 1 4 MS, MSO: the analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. E sU: serial dilution exceeds the control limits. H 148, E81, E82, E03: Batch QC is greater than reporting limit or had a negative instrument reading lower Chan the absolute value of the reporting limit. N lis, MSD: Spike recovery exceeds the upper or lower control limits. W AS(GFAA) Post.-digestion spike was outside 85-115% control Limits. Organic Qualifiers (Q - column) u Analyte was not detected at or alcove the reporting limit. NO Compound not detvcted. J Result Is an estimated value below the reporting Limit or a tentatively Identified compound (TIC). Q Result was qualitatively confirmed, but not quantified. c Pesticide identification was confirmed by GC/MS. Y The chromatographic response resembles a typical fuel pattern. z The chromatographic response does not resemble a typical fuel pattern. 8 Result exceeded calibration range, secondary dilution required. F AFCEE:Reault is an estimated value below the reporting Limit or a tentatively identified compound (TIC) organic FLags (Flags Column) 8 MB: Batch QC is greater than reporting limit. * LCE, LCD, ELC, ELQ, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lower control limits. EBI, E82, E83, MLE: Batch 4C is greater than reporting Limit A Concentration exceeds the instrument calibration range or below the reporting limit. B Compound was found in the blank and sample. 0 surrogate or matrix spike recoxories were not obtained because the extract was diluted for analysis; alto compounds analyzed at a dilution witl be flagged with a D. H Alternate peak selection upon analytical review I Indicates the presence of an interfenee, recovery is not calculated, M Manually integrated compound. P The lower of the two values is reported when the % difference between the tosults of two GC Columns is greater than 25%. Page 6 r l