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i <br /> CASE NARRATIVE <br /> GC TFH GASOLINE/PURGEABLE AROMATICS <br /> QAL Lab Reference No./SDG. : RB425 <br /> Project: Del Monte Disco <br /> lI. RECEIPT <br /> No exceptions were encountered unless a Sample Receipt Exception Report is <br /> attached to the Chain-of-Custody included with this data package. <br /> II. HOLDING TIMES <br /> A. Sample Preparation: All holding times were met. <br /> B. Sample Analysis: All holding times were met. <br /> III. METHOD <br /> Preparation: SW-846 5030A <br /> Cleanup: N/A <br /> Analysis: California LUFT Gasoline, 5/88 / SW-846 8020A(MOD) <br /> IV. PREPARATION <br /> Sample preparation proceeded normally. <br /> V. ANALYSIS <br /> A. Calibration : All acceptance criteria were met. <br /> B. Blanks: All acceptance criteria were met. <br /> C. Surrogates: All acceptance criteria were met. <br /> D. Spikes: All acceptance criteria were met. <br /> E. Samples: Sample RB425006 (MW-2) was analyzed on a diluted basis due <br /> to the concentration of target analytes. Sample RB425006 (MW-2) was <br /> then reanalyzed on a further diluted basis in order to obtain a <br /> detector response within the linear calibration range of the <br /> instrument. The results of bath analyses are included for your <br /> information. Reporting limits have been adjusted accordingly. <br /> I certify that this data package is in compliance with the terms and conditions <br /> agreed to by the client and QAL, Inc. , both technically and for completeness, <br /> except for the conditions noted above. Release of the data contained in this <br /> hardcopy data package has been authorized by the Laboratory Manager or designated <br /> person, as verified by the following signature. <br /> SIGNED: ATE; <br /> Brian Geers <br /> Manager, Organics Department <br /> kd1.043 <br /> Quality Analytical 5090 Caterpillar Road, 976244-5227 O O <br /> Laboratories Inc. Redding,CA 96003-1412 Fax No.916 244-4109 <br />