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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htW://www.mccampbell.com E-mail:main@mccampbell.com <br /> Date Sampled:07/20/98 <br /> Advanced GeoEnvironmental Client Project ID:Fire Station#3 <br /> Date Received:07/22/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact: Bill Little Date Extracted: 07/22-07/24/98 <br /> Client P.O: Date Analyzed: 07/24-07/26/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92523 <br /> Client ID M W 1-35 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Ac ` 'etone ND<30 Ethylbenzene ND <br /> -� Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chloride"' ND<10 <br /> n-Butyl benzene ND Methyl ethyl ketone" ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'9 ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> r Chlorobenzene ND Styrene` ' ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Cbloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND<10 <br /> Chloromethane ND Toluene" 7.1 <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br /> Dibromochloromethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Tiimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate""' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride"" ND <br /> 1,1-Dichloroethene ND Xylenes,total '°' 6.6 <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 1,1-Dichloropropene ND Surrogate Recoveries(IX,) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 105 <br /> W trans-1,3-Dichloropropene ND Toluene-d8 102 <br /> Ethylene dibromide ND 4-Bromotluorobenzene 115 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (1) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> �+ this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 // Edward Hamilton,Lab Director <br /> ,r <br />