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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> him//www mecampbell co m E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Gaurdino&Crawford Date Sampled 08/24/01 <br /> 837 Shaw Road Date Received 08/28/01 <br />' Stockton,CA 95215 Client Contact Paul Dotson Date Extracted 08128-08/29101 <br /> Client P O Date Analyzed 08128-08129/01 <br /> Seven Oxygenated Volatile Orgames By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 76168 76169 <br /> MW51 MW6/ Reporting Limit <br /> Client ID 082401 082401 <br />' Matrix W W S W <br /> Compound Concentration* ug/kg ug/L <br /> ' Di-isopropyl Ether(RIPE) ND ND 50 10 <br /> Ethyl tert-Butyl Ether(F-TBE) ND ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) ND ND 50 10 <br /> tent-Amyl Methyl Ether(TAME) ND ND 50 10 <br /> ' tert-Butanol ND ND 25 so <br /> ' Methanol ND ND 2500 500 <br /> Ethanol ND ND 250 50 <br /> Surrogate Recoveries(%} <br /> 1 Dibromofluoromethane 113 112 <br /> ' Comments <br /> ' *water samples are reportcd to ug1L,soil and sludge samples m ug/kg,wipes cn ug/wipe and all TCLP/STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water imrmscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> ' high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />