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110 2nd Avenue South,WD7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamnbell com E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Gardino&Crawford Date Sampled 07/29/99 <br /> 4005 North Wilson Way (G&C) Date Received 07/30/99 <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 08/04/99 <br /> [Client P O Date Analyzed 08/04/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 16336 16337 16338 16339 <br /> Reporting Limit <br /> Client ID MW-4 MW-3 MW-2 MW-1 <br /> Matrix W W W W S W <br /> Compound Concentration" uglkg ug/L <br /> Di-isopropyl Ether(D1PE) ND ND ' ND ND<35 so 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND ND<35 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND 11 330 so 1 0 <br /> tent-Amyl Methyl Ether(TAME) ND ND ND ND<35 50 1 0 <br /> Cert-Butanol ND ND ND ND<180 25 5 0 <br /> Surrogate Reco-,cries(%) <br /> Dibromofluoromethane 104 103 103 104 <br /> Comments <br /> 'water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/aipe and all TCLP 1 STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />