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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No H3092207 Date 10/02/2003 Page 6 <br /> Project Name CONNELL MOTORS Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-8D Lab Samp ID 6129-6W <br /> Descr/Location MW-8D Rec'd Date 09/23/2003 <br /> Sample Date 09/20/2003 Prep Date 09/28/2003 <br /> Sample Time 0850 Analysis Date 09/28/2003 <br /> Matrix Water OC Batch VWMS-9283 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pic Dil <br /> Methyl-tert-butyl ether(MTBE) 0 289 05 MRL ND UGIL 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL 0:82 UGIL 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL 37 UGIL 1 <br /> 1,2-Dichloroethane 162 10 MRL 430 UGIL 20 <br /> 1,2-Dibromoethane 0 092 05 MRL ND UGIL t <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 76-129 SLSA 101% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 103° 1 <br /> Approved by a2 Date <br />