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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H3102210 Date 11/03/2003 Page 3 <br /> Protect Name CONNELL MOTORS Analysts Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW 10@45- Lab Samp ID 6251-2S <br /> Descr/Location MW10Q45' Recd Date 10/23/2003 <br /> Sample Date 10/20/2003 Prep Date 10/29/2003 <br /> Sample Time 0000 Analysis Date 10/30/2003 <br /> Matrix Soil QC Batch VSMS-0293 <br /> Basis Wet Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dd <br /> Methyl-tert-butyl ether(MTBE) 14 10 PQL ND UG/KG 1 <br /> Ethyl tent-butyl ether(ETBE) 010 10 PQL ND UG/KG 1 <br /> tert-Amyl methyl ether(TAME) 013 10 PQL ND UG/KG 1 <br /> Di-isopropyl ether(DIPE) 020 10 PQL ND UG/KG 1 <br /> tert-Butyl alcohol (TBA) 70 800 PQL ND UG/KG 1 <br /> 1,2-Dichloroethane 023 10 PQL ND UG/KG 1 <br /> 1,2-Dibromoethane 1 039 10 PQL i ND UG/KEG I <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 70-130 SMSA 719% 1 <br /> 1,2-Dichloroethane-d4 70-130 SMSA 663% 1 1 <br /> Approved byL'2---- Date <br />