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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No H3102210 Date 11/03/2003 Page 5 <br /> Project Name CONNELL MOTORS Analysis Volatile Organic Compounds by GCIMS Fuel <br /> 7 Project No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW10@55' Lab Samp ID 6251-4S <br /> Deser/Location MW10@55' Recd Date 10/23/2003 <br /> Sample Date 10/20/2003 Prep Date 10/29/2003 <br /> Sample Time 0000 Analysis Date 10/30/2003 <br /> Matrix Soil QC Batch VSMS-0293 <br /> Basis Wet Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 14 10 PQL ND UG/KG 1 <br /> Ethyl tert-butyl ether(ETBE) 010 10 PQL NO UG/KG 1 <br /> tert-Amyl methyl ether(TAME) 013 10 PQL NO UG/KG 1 <br /> Di-isopropyl ether (DIPS) 020 10 PQL NO UG/KG 1 <br /> ten-Butyl alcohol (TBA) 70 800 PQL NO UG/KG 1 <br /> 1,2-Dichioroethane 023 10 PQL NO UG/KG 1 <br /> 1,2-Dibromoethane 1 039 10 PQL ND UG/KG t <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 70-130 SMSA 970% 1 <br /> 1,2-Dichloroethane-d4 70.130 SMSA 933% 1 <br /> Approved by 1 '�/� __— Date <br />