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M <br /> Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H3102210 Date 11/0312003 Page 1 <br /> Protect Name CONNELL MOTORS Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW10@100' Lab Samp ID 6251-13S <br /> Descr/Location MW10C100' Rec'd Date 10/23/2003 <br /> Sample Date 10/22/2003 Prep Date 10/29/2003 <br /> Sample Time 0000 Analysis Date 10/30/2003 <br /> Matrix Soil QC Batch VSMS-0293 <br /> Basis Wet Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dif <br /> Methyl-tent-butyl ether(MTBE) 14 10 PQL ND UG/KG 1 <br /> Ethyl tert-butyl ether(ETBE) 010 10 PQL ND UG/KG 1 <br /> tert-Amyl methyl ether(TAME) 013 10 PQL ND UG/KG 1 <br /> Di-isopropyl ether (DIPS) 020 10 PQL ND UG/KG 1 <br /> tent-Butyl alcohol (TBA) 70 800 PQL ND UG/KG 1 <br /> 1,2-Dichloroethane 023 10 PQL ND UG/KG 1 <br /> 1,2-Dibromoethane 1 039 10 PQL ND UG/KG t <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 70-130 SMSA 819° 1 <br /> 1,2-Dichloroethane-d4 70-130 SMSA 781% 1 <br /> Approved by Date <br />