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BSKANALYTICAL <br /> LABORATORIES <br /> Ery Rlfenbur Certificate of Analysis <br /> g Y <br /> Foothill Englneenng ELAP Certif eate#1180 <br /> 12793 Paddy Creek Lane Report issue Date 04/11/2003 <br /> Lodi, CA 95240 <br /> BSK Submission #: 2003031257 <br /> BSK Sample ID # 304047 <br /> Project ID Project Desc Connell Motor Truck <br /> Submission Comments <br /> Sample Type Liquid Date Sampled 03/20/2003 <br /> Sample Description CPT5 at 61 Time Sampled 1200 <br /> Sample Comments Date Received 03/20/2003 <br /> Organics Prep Analysts <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 42000 1ig/L 50 200 10000 03/29/03 03/29/03 <br /> Benzene EPA 8020 860 µg/L 03 200 60 03/29/03 03/29/03 <br /> Ethylbenzene EPA 8020 1200 µglL 03 200 60 03/29/03 03/29/03 <br /> Toluene EPA 8020 ND µg/l, 03 200 60 03/29/03 03/29/03 <br /> Total Xylenes EPA 8020 6200 gg/L 03 200 60 03/29/03 03/29/03 <br /> 1,2-Dibromoethane EPA 8260 ND ltg/L 50 40 200 04/03/03 04/03/03 <br /> 1,2-Dichloroethane EPA 8260 340 µg/L 50 40 200 04/03/03 04/03/03 <br /> Di-isopropyl Ether EPA 8260 ND gg/L 50 40 200 04/03/03 04/03/03 <br /> Ethyl t-Butyl Ether EPA 8260 ND µg/L 50 40 200 04/03/03 04/03/03 <br /> Methyl-t-Butyl Ether EPA 8260 ND Rg/L 50 40 200 04/03/03 04/03/03 <br /> t-Amyl Methyi Ether EPA 8260 ND Rg/L 50 40 200 04/03/03 04/03/03 <br /> tert-Butyl Alcohol EPA 8260 ND µg/L 50 40 2000 04/03/03 04/03/03 <br /> Surrogate <br /> - - - - --- - ---- ---- -- - -- - - - --- --- - -- -- --- -- -- -- - - ------ - - -- -- - - - - - <br /> Fluorobenzene EPA 8020 861 %Rec. 200 N/A 03/29/03 03/29/03 <br /> Toluene-d8 EPA 8260 1054 %Ree - 40 NIA 04/03/03 04/03/03 <br /> . mg/L Milligrams/Liter(ppm) PQL Practical Quantitation Limit H Analyzed outside of hold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result <br /> Rg/L Micrograms/Liter(ppb) PQL.x Dilution S Suspect result See Cover Letter for comments <br /> Rg/Kg Micrograms/Kilogram(ppb) ND None Detected at DLR E Analysis performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> Report Authentication Code Page 6 of 18 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />