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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> BSK Analytical Laboratories Client Project ID 2003031257 Sampled See Below <br /> 1414 Stanislaus Street Client Project Name Connell Motor Truck Received 03-28-03 <br /> Fresno CA 93706 Reference Number 5604 Extracted 03-31-03 <br /> Attn Miyuki Fupta Sample Description Water Analyzed 03-31-03 <br /> Sample Prep/Analysis Method EPA 5030/8260 Reported 04-01-03 <br /> Lab Numbers 5604-6W,7W, 8W <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GCIMS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID <br /> CPT4 @ 82' CPT3 @ 104' CPT3 @ 80' <br /> 304051 304052 304053 <br /> (pg/L) !L !L IL <br /> FUEL OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 ND ND ND <br /> Di-isopropyl Ether (DIPS) 0 50 063 ND ND <br /> Ethyl tert-Butyl Ether (ETBE) 050 ND ND ND <br /> tert-Amyl Methyl Ether(TAME) 0 50 ND ND ND <br /> tert-Butanol(TBA) 20 22 25 ND <br /> I <br /> VOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1,2-DCA) 050 130 68 25 <br /> Ethylene Dibromide (EDB) 050 ND ND ND <br /> Report Limit Multiplication Factor 1 1 1 <br /> Report Limit Multiplication Factor for 1,2-DCA 5 2 <br /> Date Sampled 03-19-03 03-18-03 03-18-03 <br /> Surrogate Recoveries <br /> 1,2-Dichloroethane-d4 119% 110% 128% <br /> Toluene-d8 883% 840% 956% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (Ng/L)= micrograms per liter or per billion(ppb) <br /> ANALYST APPROVED B5Jam <br /> Clary J Cone C Phillips <br /> atory Director <br />