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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2O61205 Date 06/19/2002 Page 3 <br /> Project Name CONNELL MOTORS Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-3 Lab Samp ID 30276-010 <br /> Deser/Location MW-3 Recd Date 06/12/2002 <br /> Sample Date 06/10/2002 Prep Date 06/17/2002 <br /> Sample Time 1455 Analysis Date 06/17/2002 <br /> Matrix Water QC Batch WMS31596 <br /> Basis Not Filtered Notes BH <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Did <br /> Methyl-tert-butyl ether(MTBE) 3 50 PQL ND UG/L 10 <br /> Ethyl tert-butyl ether(ETBE) 5 50 PQL ND UG/L 10 <br /> Cert-Amyl methyl ether(TAME) 3 50 PQL ND UG/L 10 <br /> Di-isopropyl ether(DIPS) 5 50 PQL ND UG/L 10 <br /> tert-Butyl alcohol (TBA) 110 200 PQL ND UG/L 10 <br /> 1,2-Dichloroethane 3 50 PQL ND UG/L 10 <br /> 1,2-Dibromoethane 1 5 50 PQL ND UG/L 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65.135 SMEA 108% 1 <br /> Toluene-d8 77-150 SMEA 111% 1 <br /> Dibromofluoromethane 57-156 SMEA 107% 1 <br /> BH Reporting limits raised due to high level of non-target analytes <br /> i <br /> Approved Dy uate <br />