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Entech Analytical Labs, Inc. CA FLAP# 2346 <br /> 525 Del Rey Avenue, Sulte E • Sunnyvale, CA 94085 • (408) 735-1550 • Fax (408) 735-1554 <br /> Sherwood Labs Corporation Date 9/28/00 <br /> Date Received 9/20/00 <br /> P.O.Box 937 Project Name Connell Truck <br /> Hilmar,CA 95324 Project Number <br /> Attn: Viclu Hubis P O Number <br /> Sampled By Client <br /> Certified Analytical Report <br /> Order ID. 22342 Lab Sample ID: 22342-006 Client Sample ID MW 7 @45' <br /> Sample Time: Sample Date: 9/18100 Matrix. Solid <br /> Parameter Result Flag DF PQL DLR Units Analysis Date QC Batch 11D Method <br /> Dusopropyl Ether ND 1 5 5 µg/Kg 9/28/00 SMS1000926 EPA 826013 <br /> Ethyl-t-butyl Ether ND 1 5 5 jig/Kg 9/28/00 SMS1000926 EPA 8260B <br /> Methyl-t-butyl Ether ND 1 5 5 gg/Kg 9128/00 SMS1000926 EPA 8260B <br /> Leri-Amyl Methyl Ether ND 1 5 5 µg/Kg 9/28/00 SMS 1000926 EPA 8260B <br /> tert-Butanol ND 1 20 20 µg/Kg 9/28/00 SMS 1000926 EPA 8260B <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromofluorobenzene 125 65- 135 <br /> Dtbromofluoromethane 136 65- 135 <br /> Toluene-d8 103 65- 135 <br /> Comment Surrogate recovery out of control limits due to matrix interference <br /> 0 <br /> ODF=Dilution Factor ND=Not Detected DLR m Detection Limit Reported PQL=Practical Quantitation LirTrit <br /> Analysts performed by Entech Analytical Labs,Inc (CA ELAP##2346) <br /> Michelle derson, Laboratory Director Environmental Analysis Since 1983 Page 6 of 19 <br />