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Entechlabs, Inc. CA 1:1_AP# 2346 <br /> 525 Def Re}/ ,avenue, Suite E * Sunnyvale, CA 94085 • (408) 735-1550 • Fax (408) 735-1554 <br /> Sherwood Labs Corporation Date 9/26/00 <br /> P-O Bog 937 Date Received 9/18/00 <br /> Hilmar,CA 95324 Project Name Connell Truck <br /> Attu Vicki Hubts ProjectNumber <br /> 0 Number <br /> Certified Analytical Report Sampled By Client <br /> Order ID: 22308 Lab Sample ID 22308-006 Client Sample ID- MW-5@45 <br /> Sample Time. Sample Date. 9/13100 Matrix Solid <br /> Parameter Result Flag DF PQL DLR Units Analysts Date QC Batch tD Method <br /> Dusopropyl Ether ND 10 5 50 µg/Kg 9/24/00 SMS2000922A EPA 8260B <br /> Ethyl-t-butyl Ether ND t0 5 50 pg/Kg 9/24/00 SMS2000922A EPA 8260B <br /> Methyl-t-butyl Ether ND 10 5 50 pg/Kg 9/24/00 SMS2000922A EPA 8260B <br /> tert-Amyi Methyl Ether ND 10 5 50 µg/Kg 9/24/00 SMS2000922A EPA 8260B <br /> tert-Butanol ND 10 20 200 pg/Kg 9/24/00 SMS2000922A EPA 8260B <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromofluorobenzene 639 65- 135 <br /> Dibromofluoromethane 108 65- 135 <br /> Toluene-d8 136 65- 135 <br /> Comment Surrogate recovery out of control limits due to matrix interference <br /> Comment Sample diluted due to high concentrations of non-target hydrocarbons <br /> i <br /> ODF=Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysts performed by Entech Analytical Labs,Inc (CA FLAP#2346) <br /> Miche �erson, Laboratory Director Environmental Analy515 51nCe 198.E Page 6 of 37 <br />