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Enviro — Chem, Inc. <br /> 1214 E. Lexington Avenue, Pomona, CA 91766 Tel (909) 590-5905 Fax (909) 590-5907 <br /> LABORATORY REPORT <br /> CUSTOMER: Pacific Titan, Inc. <br /> 17 Commercial Avenue <br /> Riverside, CA 92507 <br /> (951)780-2070 Fax(951)788-2077 <br /> PROJECT: Nustar / Job #3983 <br /> MATRIX:SOLID DATE RECEIVED:05/25/11 <br /> DATE SAMPLED:05/25/11 DATE ANALYZED:05/25-26/11 <br /> REPORT TO:MR, JACK BOYD DATE REPORTED:05/26/11 <br /> --------------------------------------- <br /> SAMPLE I.D. : Nustar #3983 Spent Abrasive <br /> LAB I.D. : 110525-61 <br /> TCLP-METALS ANALYSIS (PER 40 CFR 261.24) <br /> CONCENTRATION UNIT: MG/L IN LEA KATE <br /> "-- <br /> EPA <br /> PARAMETER RESULT PQL DF EPA# LIMIT@ METHOD <br /> ARSENIC (As) NO 0.01 1 D004 5,Q 6010B <br /> BARIUM (Ba) 0.472 0.10 1 DOD-5- 100. 0 6010B <br /> CADMIUM (Cd) ND 0 O1 I D006 1. 0 6010B <br /> CHROMIUM (Cr) 4,43 0.01 I DOIQ7 S n 6Ql0B <br /> LEM Ub) ND 0.01 1 D008 5.0 6010E <br /> MERCURY (Hg) kip 0.01 —1 D009 0 2 7470A <br /> SELENIUM (Se) No LIQ 1 DO10 0 60108 <br /> SILVER (Ao) ND 0.02 1 D011 5 0 60108 <br /> COMMENTS <br /> MG/L - Milligram per Liter - PPM <br /> TCLP Extraction Method = EPA 1311 <br /> DF Dilution Factor <br /> PQL = Practical Quantitation Limit <br /> Actual Detection Limit = PQL X DF <br /> ND = Below the Actual Detection Limit or non-detected <br /> EPA# = The EPA Hazardous Waste Number <br /> LIMIT@ = The "EPA Acceptable Land Disposal Limit" <br /> *** = The concentration exceeds the TCLP Limit (if marked) <br /> Data Reviewed and Approved by: <br /> CA.L-DHS ELAP CERTIFICATE No. ; 1555 <br />