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M <br /> M <br /> 0 i i i' i i4r i <br /> QA/ Keport <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> t.111olle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H3090301 Date: 091'1212003 Page= 21 <br /> QC Batch: VWMS-9093 Project Name: Lab Generated or Non COE Sample <br /> Matrix: Water Project No.: Lab Generated or Non COE Sample <br /> Lab Samp 1D: VWMS-9093 Field ID. Lab Generated or Non COE Sample <br /> Basis: Not Filtered Lab Ref ID: 6041-4WQ <br /> Acceptance <br /> Analysis Spike Level Sample Spice Result % Recoveries Criteria <br /> Analyte Method MS DMS Result MS DMS Units MS DMS RPD % Rec RPD <br /> 1,2-Dibromoethane 8260FA 2.50 2,60 ND 2.81 2.65 UGIL 112 106 5.5 127-76 MSA 20MSP <br /> 1,2-Dichloroethane 8260FA 2.5 2.8 Q07 2.17 2.46 UGIL 64.0 95.6 13 124.70 MSA 201-SP <br /> Dkisopropyl ether(DIPE) 8260FA 2.5 2,6 Q05 3.21 2.63 UGIL 126 103 20 15151 MSA 20LSP <br /> Ethyl tett-butyl ether(ETBE) 8260FA 2.50 2,60 ND 3.04 2.62 UGIL 122 105 15 13857 MSA 20LSP <br /> Methyl-tert-butyl ether(MTBE) 8260FA 2.6 2.6 0..26 2.08 2.15 UGIL 72.8 75,6 3.8 12762 MSA 20LSP <br /> tart-Amyl methyl ether(TAME) 8260rA 2.6 2A Q02 3,16 2.64 UGIL 1261 105 18 122-60 MSA 20LSP <br /> tent-Butyl aloohoi(TBA) 8200FA _ '16.0 70M 4.30 46.13 54.90 UGIL 55.8 67.5 19 168-42 MSA 20LSP <br /> 1,2-Dichloroethane-d4 8260FA - WE �y I OF 64.7 84.7 86.1 PERCENT 84.7 85.1 1.6 141-63 SMSA 20SM3fP <br /> Toluene-d8 8260FA IV). 1U0. 16,4 101.9 93.1 IPERCENT 102 93.1 9.1 129-76 SMSA 20SMSP <br />