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Castle Analytical Laboratory,Atwater, CA <br /> ' Lab Report No.: H3052005 Date: 05/30/2003 Page: 5 <br /> 1 Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-4 Lab Samp ID: 5751-4W <br /> Descr/Location: MW-4 Recd Date: 05/2012003 <br /> Sample Date: 05/1912003 Prep Date: 05/2712003 <br /> ' Sample Time: 1140 Analysis Date: 05127/2003 <br /> Matrix: Water QC Batch: VWMS-5273 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 1.445 2.5 MRL 46 UG/L 5 <br /> Ethyl tent-butyl ether(ETBE) 0.084 0.5 MRL 1.2 UGIL 1 <br /> Cert-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 0.155 0.5 MRL ND UG/L 1 <br /> tent-Butyl alcohol (TBA) 6.79 20. MRL ND UGIL 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL ND UG/L 1 <br /> 1,2-Dibromoethane 1 0.092 0.5 MRL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 103% 1 <br /> 1,2-Dichloroethane-d4 53.141 SLSA 100% 1 <br /> Approved by: Date: <br /> l <br />