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I <br /> Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No.: H3052005 Date: 05/30/2003 Page: 7 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> I <br /> ' Field ID: MW-6 Lab Samp ID: 5751-8W <br /> Descr/Location: MW-6 Recd Date: 05/20/2003 <br /> Sample Date: 05/19/2003 Prep Date: 05/27/2003 <br /> ' Sample Time: 1059 Analysis Date: 05/27/2003 <br /> Matrix: Water OC Batch: VWMS-5273 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units <br /> Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 2.89 5.0 MRL 95. UGIL 5 <br /> ' Ethyl tent-butyl ether(ETBE) 0.084 0.5 MRL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0.155 0.5 MRL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 8.79 20. MRL ND UGIL 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL ND UGIL 1 <br /> 1,2-Dibromoethane 0.092 0.5 MRL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 101% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 104% 1 <br /> 1 <br /> I <br /> ' Approved by: <br /> Date: <br />