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I <br />` Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3021709 Date: 02127/2003 Page: 6 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> ' Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-5 Lab Samp ID: 33384-005 <br /> Descr/Location: MW-5 Recd Date: 0211912003 <br /> Sample Date. 02114/20113 Prep Date: 02/20/2003 <br /> ' Sample Time: 1204 Analysis Date: 02/20/2003 <br /> Matrix: Water QC Batch: WMS11943 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.3 1. PQL 26. UGIL 1 <br /> ' Ethyl tent-butyl ether(ETRE) 0.5 5. PQL ND UGIL 1 <br /> Cert-Amyl methyl ether(TAME) 0.3 5. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 4.6 10. PQL ND UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 113% 1 <br /> Toluene-d8 77-150 SMEA 122% 1 <br /> 0(:!AZ: <br /> ibromofluoromethane 57-156 SMEAAZ 3.7% ! 1 <br /> Surr, recovery outside of acceptance limits clue to matrix interf. <br /> 1 <br /> Approved by: - _ -•— Date: f� <br /> 1 <br />