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i <br /> . ATTACHMENT V <br /> WELL SAMPLING,DECONTAMINATION,AND LABORATORY PROCEDURES <br /> Sampling Procedures <br /> Sampling equipment is thoroughly cleaned prior to each sample. The sampling procedure for each well <br /> includes measuring the water level and checking for the presence of separate-phase hydrocarbons (SPH), <br /> using either an electronic indicator and a clear Teflon@ bailer or an oil-water interface probe. If the <br /> measured water level in the well is below the top of casing elevation, the well may be sampled without <br /> purging. For non-purge wells, one set of water quality parameters are collected and the well is sampled <br /> with a disposable bailer. Wells not containing SPH that do not qualify as non-purge wells are purged of <br /> approximately three casing volumes of water (or to dryness) using a submersible pump, centrifugal <br /> pump, gas displacement pump, or bailer. The optimal purging rate is approximately 1 gallon per minute. <br /> The equipment and purging methods used for the current sampling event are noted on the attached field <br /> data sheets. During purging, temperature, pH, electrical conductivity, and dissolved oxygen are <br /> monitored in order to document that these parameters are stable prior to collecting samples. After <br /> purging, water levels are allowed to partially recover. Groundwater samples (both purge and no-purge) <br /> are collected using a clean disposable TeflonO bailer, placed into appropriate EPA-approved containers, <br /> labeled, logged onto chain-of-custody documents, and transported on ice to a State of California-certified <br /> laboratory. <br /> Decontamination Procedures <br /> Prior to sampling each well, reels and pumps are decontaminated with a steam cleaner. Sensitive <br /> equipment such as the water level sounder are sprayed with a non-phosphate soap and deionized water <br /> solution and rinsed with deionized water. All water used for equipment decontamination is collected and <br /> contained in a truck-mounted water tank. <br /> Laboratory Procedures <br /> The groundwater samples are analyzed for the presence of TPHg, benzene, toluene, ethylbenzene, <br /> xylenes (total), and MtBE using EPA Methods 8015 (modified) and 8021, and fuel oxygenates using <br /> EPA Method 826013. The methods of analysis for the groundwater samples are documented in the <br /> certified laboratory analytical report. <br />