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' Analytical Data <br /> Client: Earth Tech, Inc. Job Number: 720-14844-1 <br /> Client Sample ID: IDW-061908-S01 <br /> Lab Sample ID: 720-14844-1 Date Sampled: 06/19/2008 1343 <br /> Client Matrix: Solid Date Received: 06/19/2008 1443 <br /> ' 8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS) <br /> Method: 8270C Analysis Batch: 720-37270 Instrument ID: Sat 2K1 <br /> Preparation: 3550B Prep Batch: 720-37157 Lab File ID: d:\data\200806\062408\720- <br /> Dilution: 1.0 Initial Weight/Volume: 30.12 g <br /> Date Analyzed: 06/25/2008 0014 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/23/2008 1506 Injection Volume: 1.0 uL <br /> ' Analyte _� DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> Hexachlorobenzene ND 0.067 <br /> Pentachlorophenol ND 0.33 <br /> Phenanthrene ND 0.067 <br /> Anthracene ND 0.067 <br /> Di-n-butyl phthalate ND 0.17 <br /> Fluoranthene ND 0.067 <br /> Pyrene ND 0.067 <br /> Butyl benzyl phthalate ND 0.17 <br /> 3,3'-Dichlorobenzidine ND 0.17 <br /> ' Benzo[a]anthracene ND 0.33 <br /> Bis(2-ethylhexyl)phthalate ND 0.33 <br /> Chrysene ND 0.067 <br /> Di-n-octyl phthalate ND 1.0 <br /> ' Benzo[b]fluoranthene ND 0.067 <br /> Benzo[a]pyrene ND 0.067 <br /> Benzo[k]fluoranthene ND 0.067 <br /> Indeno[1,2,3-cd]pyrene ND 0.067 <br /> Benzo[g,h,i]perylene ND 0.067 <br /> Benzoic acid ND 0.33 <br /> Azobenzene ND 0.067 <br /> Dibenz(a,h)anth racene ND 0.067 <br /> Surrogate %Rec Acceptance Limits <br /> Nitrobenzene-d5 61 21 -98 <br /> ' 2-Fluorobiphenyl 49 38-96 <br /> Terphenyl-d14 45 32- 117 <br /> 2-Fluorophenol 63 28-98 <br /> Phenol-d5 67 23- 101 <br /> 2,4,6-Tribromophenol 80 37- 114 <br /> TestAmerica San Francisco Page 9 of 30 <br />■ <br />