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I GeoAnalytncal Laboratories, Inc. 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209)572-0916 . CERTIFICATE OF ANALYSIS Report# L053-10 Oxygenates Date: 3/07/00 Date Rec'd: 2/22/00 WHF Environmental Project: Foppiano Date Started: 3/04/00 PO Box 427 Date Completed: 3/06/00 Oakdale CA 95361 PO# Date Sampled: 2/22/00 ' Sampler: Jason Cashman Sample ID Lab ID MDL Method Analyte Results Units ' B-1 ® 60' L20441 5000 8260 Methyl tertiary-Butyl Ether (MTBE) ND pg/Kg 5000 Ethanol 29000 50000 tertiary-Butanol ND 5000 Di-isopropyl ether(DIPE) ND 5000 Ethyl tertiary-Butyl Ether (ETBE) ND 5000 tertiary-Amyl Methyl Ether(TAME) ND B-1 ® 65' L20442 10 8260 Methyl tertiary-Butyl Ether (MTBE) 62 pg/Kg 10 Ethanol ND 100 tertiary-Butanol ND ' 10 Di-isopropyl ether(DIPE) ND 10 Ethyl tertiary-Butyl Ether (ETBE) ND 10 tertiary-Amyl Methyl Ether (TAME) ND 10 B-1 ® 70' L20443 250 8260 Methyl tertiary-Butyl Ether (MTBE) ND pg/Kg 250 Ethanol ND ' 2500 tertiary-Butanol ND 250 Di-isopropyl ether(DIPE) ND 250 Ethyl tertiary-Butyl Ether (ETBE) ND 250 tertiary-Amyl Methyl Ether(TAME) ND Sample diluted due to high levels of non-target analytes. i B-1 ® 75' L20444 250 8260 Methyl tertiary-Butyl Ether (MTBE) ND pg/Kg 250 - Ethanol ND ' 2500 tertiary-Butanol ND 250 Di-isopropyl ether(DIPE) ND 250 Ethyl tertiary-Butyl Ether (ETBE) ND ' 250 tertiary-Amyl Methyl Ether(TAME) ND Sample diluted due to high levels of non-target analytes. B-2 ®5' L20446 2500 8260 Methyl tertiary-Butyl Ether (MTBE) _ ND pg/Kg 2500 Ethanol ND 25000 tertiary-Butanol ND 2500 Di-isopropyl ether(DIPE) ND ' 2500 Ethyl tertiary-Butyl Ether (ETBE) ND 2500 tertiary-Amyl Methyl Ether(TAME) ND Sample diluted due to high levels of non-target analytes. 1 ' Steve Hoffmann Donna Keller Chemist Certification # 1157 Laboratory Director