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Report Number 46978 QC Report Matrix Spike/ Matrix Spice Duplicate Date 11/22/2005 Project Name Quick Stop 39 Project Number 7039.46 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 47001-05 <0 50 400 400 378 367 ug/L EPA 8260B 11121/05 945 91 8 2 88 70-130 25 Toluene 47001-05 <0 50 400 400 381 359 ug/L EPA 8260B 11/21/05 953 897 611 70-130 25 Tert-Butanol 47001-05 <5 0 200 200 193 196 ug/L EPA 8260E 11/21105 96 7 978 110 70-130 25 Methyl-t-Butyl Ether 47001-05 41 400 400 790 772 ug/L EPA 8260E 11/21105 939 896 464 70-130 25 Benzene 47011-05 <0 50 400 400 420 404 ug/L EPA 8260B 11/20/05 105 101 4 12 70-130 25 Toluene 47011-05 <0 50 40 0 400 426 406 ug/L EPA 8260B 11/20/05 106 101 4 85 70-130 25 Tert-Butanol 47011-05 <50 200 200 194 194 ug/L EPA 8260B 11/20/05 973 972 0 136 70-130 25 Methyl-t-Butyl Ether47011-05 <0 50 400 400 32 9 32 5 ug/L EPA 8260E 11/20/05 823 812 1 32 70-130 25 Benzene 47001-03 <0 50 400 400 428 41 4 ug/L EPA 8260B 11/21/05 107 103 351 70-130 25 Toluene 47001-03 <0 50 400 400 429 41 3 ug/L EPA 8260B 11/21/05 107 103 368 70-130 25 Tert-Butanol 47001-03 <5 0 200 200 201 199 ug/L EPA 82606 11/21105 101 996 0 972 70-130 25 Methyl-t-Butyl Ether 47001-03 <0 50 400 400 337 336 ug/L EPA 82606 11/21105 84 3 841 0 232 70-130 25 Benzene 46978-04 <0 50 400 400 402 391 ug/L EPA 8260E 11/19/05 100 979 264 70-130 25 Toluene 46978-04 <0 50 400 400 382 374 ug/L EPA 8260B 11/19/05 955 936 2 05 70-130 25 Tert-Butanol 46978-04 <5 0 200 200 216 217 ug/L EPA 8260B 11/19/05 108 109 0 425 70-130 25 Methyl-t-Butyl Ether 46978-04 <0 50 400 400 398 39 7 ug/L EPA 82608 11/19/05 996 99 2 0 432 70-130 25 t • KIFF ANA CAL, LLC Approved By Joe iff 2795 2nd St, Suite 300 is, CA 95616 530-297-4800