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C J r QC Report : Matrix Spike!Matrix Spike Duplicate Report Number.- 43887 Date : 5/26/2005 Project Name : Quick Stop 39 Project Number : 7039.46 Duplicate Duplicate Spiked Spike Spiked Spiked Spiked Spiked Sample Relative Spiked Sample Spike Dup. Sample Sam le Sample Sample Relative Percent Percent Parameter Sample Value Level Level Value Value Units Methods Analyzed RecOPercv. Reco .Percent Percent Limit v. emit Benzene 43943-04 <0.50 40.0 40.0 40.0 39.6 ug/L EPA 82608 5125105 99.9 99.1 0.846 70-130 25 Toluene 43943-04 <0.50 40.0 40.0 40.5 40.0 ug/L EPA 8260B 5125105 101 100 1.23 70-130 25 Tert-Butanol 43943-04 <5.0 200 200 200 204 ug/L EPA 8260B 5125105 100 102 1.65 70-130 25 Methyl-t-Butyl Ether 43943-04 0.55 40.0 40.0 38.7 38.8 ug/L EPA 8260B 5/25/05 95.4 95.7 0.339 70-130 25 Benzene 43887-01 <0.50 40.0 40.0 40.5 40.0 ug/L EPA 8260E 5123/05 101 100 1.29 70-130 25 Toluene 43887-01 9.4 40.0 40.0 49.7 49.2 ug/L EPA 82608 5/23/05 101 99.7 1.22 70-130 25 Tert-Butanol 43887-01 <5,0 200 200 197 198 ug/L EPA 82608 5/23105 98.6 98.8 0.249 70-130 25 Methyl-t-Butyl Ether 43887-01 <0.50 40.0 40.0 36.4 36.2 ug/L EPA 8260B 5123/05 91.0 90.4 0.685 70-130 25 Benzene 43887-03 <0.50 40.0 40.0 38.3 37.7 ug/L EPA 8260B 5/26/05 95.8 94.2 1.66 70-130 25 Toluene 43887-03 4.6 40.0 40.0 41.6 40.6 ug/L EPA 8260B 5/26/05 92.5 90.1 2.66 70-130 25 Tert-Butanol 43887-03 <5.0 200 200 187 186 ug/L EPA 8260B 5/26/05 93.7 92.8 0.954 70-130 25 Methyl-t-Butyl Ether 43887-03 <0.50 40.0 40.0 38.0 38.1 ug/L EPA 8260B 5/26/05 94.9 95.2 0.236 70-130 25 Benzene 43936-01 <0.50 40.0 40.0 38.0 36.8 ug/L EPA 8260E 5125/05 95.0 92.1 3.15 70-130 25 Toluene 43936-01 0.72 40.0 40.0 38.7 37.7 ug/L EPA 8260E 5/25/05 94.9 92.4 2.71 70-130 25 Tert-Butanol 43936-01 48 200 200 262 261 ug/L EPA 8260B 5/25/05 107 106 0.305 70-130 25 Methyl-t-Butyl Ether 43936-01 11 40.0 40.0 50.5 51.2 ug/L. EPA 8260B 5/25105 98,8 100 1.83 70-130 25 Benzene 43905-01 0.70 40.0 40.0 37.4 36.9 ug/L EPA 8260B 5123/05 91.7 90.6 1.24 70-130 25 Toluene 43905-01 <0.50 40.0 40.0 37.4 36.2 ug/L EPA 8260B 5/23/05 93.5 90.5 3.29 70-130 25 KIFF ANALYTICAL, LLC Approved By: Joe iff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800