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Report Number 31246 QC Report Matrix Spikel Matrix Spike Duplicate Date 2110/2003 Project Name Quick Stop #39 Project Number 7039 44 Duplicate Duplicate Spiked u P Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Value Sample Spike Sample Sample Analysis Date Percent Percent Percent Recov LiParameter Sample VauLe l Level VaueValUnits Method Analyzed Recov Recov DffLmitmit Benzene 31231-07 100 392 398 132 131 uglL EPA 8260B 215103 684 64 5 590 70-130 25 Toluene 31231-07 36 39 2 398 401 403 uglL EPA 82606 215103 931 92 2 0 977 70-130 25 Tert-Butanol 31231-07 120 196 199 324 318 uglL EPA 82608 215103 101 967 459 70-130 25 Methyl-t-Butyl Ether 31231-07 250 392 398 283 279 uglL EPA 82606 215103 94 4 81 5 14 6 70-130 25 Benzene 31221-01 <0 50 400 400 41 6 41 1 uglL EPA 8260B 214103 104 103 1 16 70-130 25 Toluene 31221-01 <0 50 400 400 38 0 377 uglL EPA 8260E 214103 951 94 3 0 844 70-130 25 Tert-Butanol 31221-01 <5 0 200 200 202 201 uglL EPA 82606 214103 101 100 0 388 70-130 25 Methyl-t-Butyl Ether 31221-01 <0 50 400 400 366 366 uglL EPA 82606 214/03 91 5 916 0 109 70-130 25 Benzene 31246-01 <0 50 400 400 39 7 38 4 uglL EPA 8260B 2/4103 99 2 961 322 70-130 25 Toluene 31246-01 <0 50 400 400 368 335 uglL EPA 82606 2/4/03 920 838 930 70-130 25 Tert-Butanol 31246-01 <5 0 200 200 195 185 uglL EPA 8260B 214103 - 974 923 536 70-130 25 Methyl-t-Butyl Ether 31246-01 <0 50 400 400 41 5 41 0 ug/L EPA 82606 214!03 104 102 1 26 70-130 25 Benzene 31323-03 500 400 400 500 470 ug/L EPA 8260B 216103 000 000 0 00 70-130 25 Toluene 31323-03 15 400 400 451 485 uglL EPA 8260B 216103 744 828 107 70-130 25 Tert-Butanol 31323-03 <5 0 200 200 203 198 uglL EPA 82606 216103 102 98 8 270 70-130 25 Methyl-t-Butyl Ether 31323-03 16 400 400 592 554 ug/L EPA 8260B 216103 109 99 6 890 70-130 25 I I i KIFF ANALYTICAL, LLC Approved By Jbel Kiff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800 t� I—