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Gec. _ nalytical Laboratories,-.tnc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> Report# P007-21 CERTIFICATE OF ANALYSIS Date: 1/10/03 <br /> Thorpe Oil Date Rec'd: 1/07/03 <br /> Date Started. 1/09/03 <br /> PO Box 357 Project S.T.Service-3505 Navy Dr. Stockton,Ca. Date Completed:1/09/03 <br /> Lodi CA 95241 <br /> Date Sampled: 1/07/03 <br /> PO# Time: <br /> Sample ID: TKl Water Sample.From Tank Pit Sampler: R.Azevedo(Geo) <br /> Lab ID: P300119 <br /> Method RL Analvte Results Units <br /> 8260B 100 Methyl tert-butyl ether(MTBE) 2120 pg/L <br /> 8000 Ethanol ND <br /> 1000 tert-Butanol ND <br /> 100 di-Isopropyl ether(DIPE) ND <br /> 100 Ethyl tert-butyl ether(ETBE) ND <br /> 100 tert-Amyl methyl ether(TAME) ND <br /> 200 Ethylene dibromide(EDB) ND <br /> 100 1,2-Dichloroet ane(1,2-DCA) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery OC Limit% <br /> 1,2-Dichloroethane-d. 1000 986 98.6 72-132 <br /> 2-Bromo-l-chloropropane 1000 966 96.6 71-134 <br /> 4-Bromofluorobenzene 1000 980 98.0 74-132 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification n 1157 Laboratory Director <br />