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CASTLE ANALYTICAL LABO 'TOR- Phone: (209)384-2O <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Fax: (209)384-1507 <br /> Certificate#fi2480 <br /> rFAtImSteve <br /> Solutions,Inc. Client Project Name:Premier Finishing <br /> Method:EPA 5030/82603 <br /> Lab Reference Number:1903100 instrument lD:VARIAN M5 <br /> Sample Description:Water Prepared: 03-29-19 <br /> 5381 p Analyzed: 03-29-19 <br /> eier Reported: 04-05-19 <br /> QUALITY CONTROL DATA REPORT <br /> $PIKE ID: VWMS-3299 <br /> Reporting BLANK Spiking ��%ItR <br /> %R <br /> Limit Result Level Limits <br /> uglL ug/L u !L <br /> MI' t <br /> DS ND 75 NA* 70-130% <br /> hol(t-BA) 10 <br /> 0.50 ND 2.5 NA* 70-130% <br /> tyl ether (MTBE) 0.50 ND 2.5 NA* 70-130% <br /> other{DIPS) 0.50 ND 2.5 NA* 70-130% <br /> l ether(ETBE) 0.50 ND 2.5NA* 70 130%hyl ether(TAME) ND 2.5 NA* 70-130% <br /> 1,2-Dichloroethane(1,2-DCA) 0.50 70-130% <br /> 0.50 ND 2.5 NA <br /> Eth Iene dibromide(EDB) 0.50 ND 2.5 NA* 70-130% <br /> 1,1-Dichloroetherne(1,t,DCE) ND 2 5 NA* 70-130% <br /> Benzene 0.50 <br /> D.SD ND 2.5 NA* 70-130% <br /> Trichloroethene(TCE) ND 25 NA* 70-130% <br /> Toluene Q•5D <br /> Chlorobenzene 0.50 ND 2.5 NA* 70-130% <br /> Surro ate: 1 D 104% 10 NA* 70-'130% <br /> Dibromofluoromethane 107% 10 NA" 70-130% <br /> 1,2-Dichloroethane-d4 1.0 <br /> 1,0 116% 10 NA* 70-130% <br /> Toluene d8 96.3% 10 NA* 70-130% <br /> 4-Bromofluorobenzene 1.0 <br /> Spiking CONTROL. CONTROL %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> u IL %R %R <br /> COIWOUNDS 85.3% 89.7% 7D-130% 4.33% <br /> t-But I Alcohol(t-BA) 75 0.0% <br /> 2,5 96.8% a86.4%/ <br /> % 70-13Q% <br /> Moth !t hutyl ether (MTBE) 2 5 108% %° 70-130% 29.4"/" <br /> Diisoprop l ether(DIPE) 111% 70-130% 24.7Ethyl t-Butyl ether(ETRE) 2 52.5101% % 70-130% 15.65% <br /> t-Am I meth I ether(TAME) 2 5 106% % 70-130% <br /> 1,2-Dichloroethane(1,2-DCA) 2,5 114% 110% 70-130% 3.21% <br /> Eth lene dibromide(EDB) 2.5 95.611A 84.4% 70-130% 12.44% <br /> 1,1-❑ichloroethene(1,1,DCE) 2.5 95.6% 98.0% 70-130% <br /> Benzene 98.4% 99,2% 70-130% <br /> Trichloroethene(TGE) 2.5 70-130% <br /> 2,5 101% 100% ° <br /> Toluene 83.6% 99.6% 70-130% 17.5/0 <br /> Chlorobenzene 2.5 <br /> Surrogate: 95.5% 70-130% 13.48% <br /> Dibromofluoromethane 10 1225%16% <br /> 109% 70-130% 14.0% <br /> hloroethane-d4 10 -124% .. .-_._.... 101% 7Q 13f}% 19.7%_ .._. . <br /> Toluene-d8 10 - 0.68% <br /> 4-Bromofluorobenzene <br /> 10 103% 103% 70-130°/a <br /> LVA*See Conh'al Sri <br /> Control Spilce Dup <br /> APPROVED BY: <br /> James C, P fillips/L oratory Director or <br /> Ciari J. Cone/Lab rafory Manager <br />