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ANALYTICAL RESULTS <br /> Total Petroleum Hydrocarbons By GC <br /> lEI/GTEL Client ID CES06CES06 <br /> ogin Number W7070538 <br /> Project ID (number) 97735 Method GC <br /> Project ID (name) CANONIE/DIESEL PERFORMANCE/MODESTO/CA Matrix Solids <br /> NEI/GTEL Sample Number W7070538-01 W7070533 02 W7070538-03 W7070538 04 <br /> Client ID OP SB1 15 0 DP SB1 30 0 DP S83-15 0 OP SB3 20 0 <br /> Date Sampled 07/23/97 07/23/97 07/23/97 07/23/97 <br /> Date Prepared 08/02/97 08/02/97 08/02/97 08/02/97 <br /> Date Analyzed 08/06/97 08/06/97 08/06/97 08/06/97 <br /> Dilution Factor 1 00 1 00 2 00 3 00 <br /> Reporting <br /> Analyte Limit Units Concentration Wet Weight <br /> TPH as Kerosene; 10 mg/kg < 10 < 10 280 470 <br /> TPH as Diesel 10 mg/kg < 10 < 10 58 77 <br /> TPH as Lubricating Oil 10 ung/fig < 10 < 10 < 20 < 30 <br /> Percent Solids -- 81 8 70 2 81 3 75 4 <br /> Notes <br /> Dilution Factor <br /> Dilution factor indicates the adjustments made for sample dilution <br /> GC <br /> 'Ytrac'-ien by 'r4 '"ethrd ^650 scnicaticn, U 11 Tethod 0332?(iodified3 is ised `cr aualitat ve identification of -vel patt=rrns Trp ce*hod -ias peen <br /> modified to include quantitation by applying calibration and quality assurance guidelines outlined in "Test Methods for Evaluating Solid Waste <br /> Physical/Chemical Methods" SW-841 Third Edition including promulgated Update 1 This method is equivalent to the Caliform a LIFT manual 111, method <br /> for diesel fuel Due to the qualitative similarities between Kerosene and Diesel Fuel the material present was quantified only as the product which it <br /> most resembled chromatographically The reporting limit for the other analyte was elevated accordingly Lubricating oil can not be qualitatively <br /> identified by type of oil because of chromatographic likeness of different oil types Due to non-volatility of certain oils much of the oil present <br /> may not be quantified by this method Quantitation obtained for lubricating oil by this method should therefore be treated as an estimate This <br /> method quantifies lubricating oil against 10-W-30 standards <br /> W7070538-03 <br /> The material present is qualitatively uncertain Therefore all material in the C9 to C16 range was quantitated against kerosene and C16 to C24 was <br /> quantitated against diesel fuel without respect to pattern <br /> W7070538 04 <br /> The material present is qualitatively uncertain Therefore all material in the C9 to Lib range was quantitated against kerosene and C16 to C24 was <br /> quantitated against diesel fuel without respect to pattern <br /> GEI/GTEL Wichita KS <br /> W7070538 Page 1 <br />