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ANALYTICAL RESULTS Total Petroleum Hydrocarbons By GC NEI/GTEL Client ID CES06CES06 gin Number W7070538 Project ID (numner) 97735 Method GC Project ID (name) CANONIE/DIESEL PERFORMANCE/MCDESTO/CA Matrix Solids NEI/GTEL Sample Number W7070538 09 W7070538 10 Client ID DP 585-15 0 DP SBS 30 0 Date Sampled 07/23/97 07/23/97 Date Prepared 08/02/97 08/02/97 Date Analyzed 08/07/97 08/07/97 - Dilution Factor 1 00 1 00 - Reporting Analyte Limit Units Concentration Wet Wel ht TPI as Kerosene 10 mg/kg < 10 < IG -- -- TPH as Diesel 10 mg/kg < 10 < 10 -- TPH as Lubricating Oil IG mgfkg < 10 < 10 -- Percent Solids % 78 1 75 4 -- -- Notes Dilution Factor Dilution factor indicates the adjustments made for sample dilution QC E(t-acon by 7A aethod 355u ksom cation) ASTM `lethod 033Mmrdified) 's used for qualitative identification of Nei pate—s re method rias peen modified to include quantitation by applying calibration and quality assurance guidelines outlined in Test Methods for Evaluating Solid Waste Physical/chemical Methods" SW-846 Third Edition including promulgated Update 1 This method is equivalent to the California LUFT manual DHS method for diesel fuel Due to the qualitative similarities between Kerosene and Diesel Fuel the material present was quantified only as the product which it most resembled chromatographically The reporting limit for the other analyte was elevated accordingly Lubricating oil can not be qualitatively identified by type of oil because of chromatographic likeness of different oil types Due to non-volatility of certain oils much of the oil present may not be quantified by this method Quantitation obtained far lubricating oil by this method should therefore be treated as an estimate This method quantifies lubricating oil against 10-W-30 standards IDEI/GTEL Wichita KS W7070538 Page 3