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t110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> hgR://www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Grewals Market Date Sampled:01123-01/24/02 <br /> 837 Shaw Road Date Received: 01/31/02 <br /> Stockton,CA 95215 Client Contact: Tim Cuellar Date Extracted:01/31-02/07/02 <br /> Client P.O: Date Analyzed:01/31-02/07/02 <br /> Seven Oxygenated Volatile Organics By W/MS <br /> EPA method 8260 modified <br /> i <br /> Lab ID 89362 89363 89364 89365 <br />' Reporting Limit <br /> Client 1D P-10/80' P-10/90' P-11/15' P-11145' <br />' Matrix S S S S 5 w <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND ND ND 5.0 1.0 <br />' Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 5.0 1.0 <br /> I <br /> Methyl tert-Butyl Ether(MTBE) ND ND ND 12 5.0 1.0 <br /> t <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> tert-ButanoI ND ND ND ND 25 5.0 <br /> Methanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 99 100 101 101 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC!SPLP extracts in ug/L <br />' ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 1 Edward Hamilton,Lab Director <br /> ��1 <br />