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Report Number 40680 } QC Report: Matrix Spike/Matrix Spike Duplicate Date 11/12/2004 Project Name Ace Tomato Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike DUD Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit TPH as Diesel 40680-02 <1 0 200 200 158 166 mg/Kg M EPA 8015 10/26/04 79 0 82 9 487 60-140 25 TPH as Diesel Blank <50 1000 1000 927 998 ug/L M EPA 8015 10/26/04 92 7 998 737 70-130 25 Benzene 40704-17 <0 0050 00398 00391 00406 00400 mg/Kg EPA 8260B 10/26/04 102 102 0138 70-130 25 Toluene 4070417 <0 0050 00398 00391 00377 00374 mg/Kg EPA 8260B 10/26/04 948 95 5 0 748 70-130 25 Tert-Butanol 4070417 <0 0050 0199 0 196 0 185 0180 mg/Kg EPA 8260E 10/26/04 930 91 9 126 70-130 25 Methykt-Butyl Ether407O4-17 <0 0050 00398 00391 00364 00365 mg/Kg EPA 8260B 10/26/04 916 932 1 79 70-130 25 Benzene 40735-01 <0 50 400 400 412 38 4 ug/L EPA 82608 10/27/04 103 95 9 7 04 70-130 25 Toluene 40735-01 <0 50 400 400 428 398 ug/L EPA 8260B 10/27/04 107 996 716 70-130 25 Ten`-Butanol 40735-01 <50 200 200 199 188 ug/L EPA 8260B 10/27/04 99 4 941 552 70-130 25 Methyl-t-Butyl Ether40735-01 <0 50 400 400 429 403 ug/L EPA 8260B 10/27/04 107 101 643 70-130 25 Benzene 40676-02 <0 50 400 400 406 397 ug/L EPA 8260B 10/27/04 101 99 2 226 70-130 25 Toluene 40676-02 <0 50 400 400 393 386 ug/L EPA 8260B 10/27/04 984 96 5 194 70-130 25 Ten`.-Butanol 40676-02 <50 200 200 193 196 ug/L EPA 8260B 10/27/04 966 978 1 16 70-130 25 Methyl-t Butyl Ether40676-02 60 400 400 109 108 ug/L EPA 8260B 10/27/04 121 118 294 70-130 25 KI FF ANALYTICAL, LLC Approved By Jo I iff 27952nd St, Suite 300 Davis, CA 95616 530-297-4800