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110 Second Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 64i//www.mccampbell coin E-mail matn@mccampbell cam <br />' Advanced GeoEnvironmental Client Protect ID #0184,Larry's Date Sampled 07/22/98 <br /> Auto Date Received 07/24/98 <br /> 4005 North Wilson Way <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08/01-08102/98 <br /> Client P O Date Analyzed 08/01-08/02198 <br />' Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 92687 <br />' Client ID VW4-7122198 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<2400 Ethylbenzene 2500 <br /> Benzene 24,000 Hexachlorobutadiene ND<1000 <br /> Bromobenzene ND<1000 Iodomethane ND<1000 <br /> Bromochloromethane ND<1000 lsopropylbenzene ND<1000 <br /> Bromodichloromethane ND<1000 p-Isopropyl toluene ND<1000 <br /> Bromofonn ND<1000 Methyl butyl ketone NIX 1000 <br /> Bromomethane ND<1000 Methylene Chlonde° ND<1000 <br /> n-Butyl benzene ND<1000 Methyl ethyl ketone' ND<1000 sec-Butyl benzene ND<1000 Methyl isobutyl ketone ND<1000 <br /> ten-Butyl benzene ND<1000 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<1000 Napthalene ND<1200 <br /> Carbon Tetrachloride NIX1000 n-Propyl benzene NIX1000 <br /> M Chiorobe izene ND<1000 Styrene ND<1000 <br /> Chloroethane ND<1000 1,1,1,2-Tetrachloroethane ND<10W <br /> 2-Chloroethyl Vinyl Eth ND<1000 1,1,2,2-Tetrachloroethane ND<1000 <br /> Chloroform ND<1000 Tetrachloroethene NIX1000 <br />' Chloromethane N13<1000 Toluene 18,000 <br /> 2-Chlorotoluene ND<10W 1,2,3-Tnchlorobenzene N13<1000 <br /> 4-Chlorotoluene ND<1000 1,2,4-Tnchlorobenzene ND<1000 <br /> Dibromochloromethane ND<1000 1,1,1-Tnchloroethane NIX1000 <br /> 1,2-Dibromo-3-chloropropane ND<1000 1,1,2-Tnchloroethane ND<1000 <br /> Dibromomethane ND<1000 Trichloroethene ND<1000 <br /> 1,2-Dichlorobenzene ND<1000 Tnehlorofluoromethane ND<1000 <br />' 1,3-Dichlorobenzene ND<1000 1,2,3-Tnchloropropane ND<1000 <br /> 1,4-Dichlorobenzene ND<1000 1,2,4-Tnmethylbenzene 1700 <br /> Dichlorodifluoromethane ND<1000 1,3,5-Tnmethylbenzene ND<1000 <br /> 1,]-Dichloroethane ND<1000 Vinyl Acetate m ND<1000 <br /> 1,2-Dichloroethane ND<1000 Vinyl Chloride ° NIX1000 <br /> 1,1-Dichloroethene ND<1000 Xylenes,total 13,000 <br /> cis-1,2-Dichloroethene ND<1000 <br /> trans-l,2-Dichloroethene NIX1000 <br />' 1,2-Dichloropropane ND<1000 <br /> 1,3-Dichloropropane ND<1000 <br /> 2,2-Dichloropropane ND<1000 Comments <br /> 1,1-Dichloropropene NIX1000 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<low Dibromofluoromethane ]03 <br /> trans-l,3-Diehloropropene ND<1000 Toluene-d8 100 <br /> Ethylene dibromide ND<1000 4-Bromofluorobenzene 112 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone, (c) (2-chioroethoxy)ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than —5 vol % <br />' sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethane,(o)dimethylbenzenes <br /> DHS Certification No 1644 / Edward Hamilton,Lab Director <br />