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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> F,4 http/lwww mecampbel]coin E-mail main@mccampbell cam <br />' <br /> Advanced GeoEnvironmental Client Project 1D #95-0184,Larry's Date Sampled 04/24/98 <br />' 4005 North Wilson Way Auto Date Received 04/28/98 <br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 04129-04/30/98 <br />' Client P O Date Analyzed 04/29-04/30198 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 88583 <br /> Client ID M W 1/4-24-98 <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone` ' ND<4 Ethylbenzene 240 <br /> Benzene 820 Hexachlorobutadiene ND<4 <br />' Bromobenzene ND<4 lodomethane ND<4 <br /> Bromochloromethane ND<4 Isopropylbenzene 18 <br /> Bromodichloromethane ND<4 p Isopropyl toluene ND<4 <br /> Bromofotnt ND<4 Methyl butyl ketone' ' ND<4 <br />' Bromomethane ND<4 Methylene Chloride"' ND<4 <br /> n Buty]benzene ND<4 Methyl ethyl ketone" ND<4 <br /> sec-Butyl benzene ND<4 Methyl isobutyl ketone`s ND<4 <br /> Cert-Butyl benzene 29 Methyl teri-Butyl Ether(MTBE) --- <br /> Carbon Disulfide 65 Naphthalene 12 <br /> Carbon Tetrachloride ND<4 n-Propyl benzene 45 <br /> Chlorobenzene ND<4 Styrene" ND<4 <br /> Chloroethane ND<4 1,1,1,2-Tetrachloroethane ND<4 <br /> I 2-Chloroethyl Vinyl Ether"' ND<4 1 1 2,2-Tetrachloroethane ND<4 <br /> Chloroform ND<4 Tetrachloroethene ND<4 <br /> Chloromethane ND<4 Toluene` 460 <br /> 2-Chlorotoluene ND<4 1,2 3-Trichlorobenzene NIX4 <br /> 4-Chlorotoluene ND<4 1,2 4 Trichlorobenzene NDV <br /> Dibromochloromethane ND<4 1,1,1 Tiiehloroethane ND<4 <br /> 1,2-Dibromo-3-chloroprOpane ND<4 1 1 2 Trichloroethane ND<4 <br /> Dibromomethane ND<4 Trichloroethene ND<4 <br />' 1 2-Dichlorobenzene ND<4 TriChIOrolluoromethan e ND<4 <br /> I 3-Dichlorobenzene ND<4 1,23-Tiichloropropane ND<4 <br /> 1,4-Dichlorobenzene ND<4 1,2,4-Trimethylbenzene 290 <br /> Dichlorodifluoromethane ND<4 1,3,5 Trnnethylbenzene 68 <br /> 1,1-Dichloroethane ND<4 Vinyl Acetate"" 10 <br /> 1,2-Dichloroethane 18 Vinyl Chloride"' ND<4 <br /> 1 1-Dichloroethene ND<4 Xylenes,Iota] j0j 940 <br /> cis-1,2-Dichloroethene ND<4 <br /> trans-1,2-Dichloroethene ND<4 <br /> 1,2-Dtchloropropane ND<4 <br /> 1,3-Dtchloropropane ND<4 <br /> 2,2-Dichloropropane ND<4 Comments <br /> l,l-Dtchloropropene ND<4 Surrogate Reco%cries(%) <br /> cis-1,3-Dtchloropropene ND<4 Dibroniolluoromethane 98 <br /> trans-1,3-Dtchloropropene ND<4 Toluene-d8 93 <br /> I Ethylene dibromide ND<4 4-Broniolluorobenzene 101 <br /> water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 uglL vapor samples 05 uglL solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) eihene, (d) 2-hea2none (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isoprapylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester (n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />