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110 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> 1 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 6 44 <br /> hitp//www mccam 2b lg l corn E-mail main@mccampbell corn <br /> 1 <br /> Advanced GeoEnvironmenta! Client Protect ID X95-0184, Larry's Date Sampled 04/24/98 <br /> 4005 North Wilson Way Auto Date Received 04/28/98 <br />' <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 04/29/98 <br />' Client P O Date Analyzed 04/29/98 <br /> Volatile Organics By GC/M1IS <br /> EPA method 8260 <br />' Lab ID 88585 <br /> Client ID MW3/4-24-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ND<I 5 Eth)lbenzene ND <br /> Benzene 8 3 He-,achlorobutadiene ND <br />' Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodrehloromethane ND p-Isopropyl toluene ND <br /> Bi ontoform ND Methyl butyl ketone' ' ND <br />' Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone" ND<1 5 <br /> sec-Bury)benzene ND Methyl isobutyl ketone'm ND <br /> tert-Butyl benzene ND Methv]tart-Butyl Ether(MTBE) --- <br /> M Carbon Disulfide 1 5 N'aphtha)ene ND <br /> Carbon TetraLlllorlde ND n-Propyl benzene 1 0 <br /> Chlorobenzene ND Styrene` ' ND <br /> Chloroethane ND 1,i,1 2-Ten achlo oethane ND <br />' 2-Chloroethyl Viny)Ether" ND 1 1 2 2 Tetrachloroethane ND <br /> Chloroform 65 Tetrachloioethene ND <br /> Chloromethane ND To]nLA1e" ND <br /> 2-Chlorotoluene ND 1,2 3-Trichloroben2ene ND <br />' 4-Chlorotoluene ND 12,4-Trichlorobenzene ND <br /> Dibiomoch)oromethane ND 1,1 1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 11,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br />' <br /> 1,2 Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND l 2 3-Tiichloropiopane ND <br /> 1,4-Dichlorobenzene ND 1,2 4 Tnmethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3 5-Trimethylbenzene ND <br />' 1,1 Dichloroethane ND Vinyl Acetate""' 1 i <br /> 1,2-Dichloroethane 4 1 Vinyl Chloride"" ND <br /> 1,1-Dichloi oethene ND X)lanes total '°' ND <br /> cis-1,2-Dichloroethene ND <br />' trans 1,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br />' 2,2-Dichloropropane ND Coirinttnts <br /> l,1-Dichloropropene ND Surrogate Recot cries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 94 <br /> trans-I3-Dichloropropene ND Toluene-d8 100 <br /> Ethylene dibromide ND 4 Brontofluorobenzene 107 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,a ipes in ug/.t rpe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor Samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/tsipe ND means not detected abote the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-heeanone (e) dichloromethane (t) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than eater immiscible sheen is present (r) liquid sample that contacts greater than --5 vol % <br /> sediment 0)sample diluted due to high organic content (k)peaks piestnt in this carbon range do not)hatch the patten)of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethane,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />