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1 ` <br /> 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ht //www mccam bell cam E-mail math@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID #95-0184, Larry's Auto Date Sampled 04/24/98 <br />' 4Date Received 04/28/98 <br /> 005 North Wilson Way <br /> Client Contact Kevin McKibben Date Extracted 04124-04/30/9$ <br /> Stockton,CA 95205 <br />' Client P O Date Analyzed 04129-04/30/98 <br /> Volatile Organics By GC/AIS <br /> EPA method 8260 <br />' Lab ID 88592 <br /> Client ID VWSC/4-24-98 <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone` ND<570 Ethylbenzene 2000 <br /> Benzene 7600 Hexachloiobutadmic ND<170 <br />' Bromobenzene ND<170 lodomethane ND<170 <br /> Bromochloromethane ND<170 lsopropylbenzene ND<170 <br /> Bromodichloromethane ND<170 p Isopropyl toluene ND<170 <br /> Bromoform ND<170 Methyl butyl ketone' ' ND<170 <br />' Bromomethane ND<170 Methylene Chloride" ND<270 <br /> n-Butyl benzene ND<170 Methyl ethyl ketone" ND<170 <br /> sec-Butyl benzene ND<170 Methyl uobutyl ketone'K ND<l70 <br /> tert-Butyl benzene ND<170 Methyl Cert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<170 Naphthalene 650 <br /> Carbon Tetrachloride ND<170 n Propyl benzene 310 <br /> ClilorooenLene ND<170 Styrene" ND<170 <br /> Chloroethane ND<170 l 1,1,2-Teti achloroethane ND<170 <br />' 2 Chloroethyl Vinyl Ether" ND<170 1 1 2 2-Teti achloroethane ND<170 <br /> Chloroform ND<170 Tetrachloroethene ND<170 <br /> Chloromethane NID<170 Toluene` 12,000 <br /> 2-Chlorotoluene ND<170 1,2,3 Trichlowbenzene ND<170 <br />' 4-Chlorotoluene ND<170 1,2,4-Trichiorobenzene ND<170 <br /> Dibromochloromethane NIX170 1,1,1-Trichloroethane ND<170 <br /> l2-Dibromo-3-chloropropane NIX170 1,12-Trichloroethane ND<170 <br /> Dibromomethane ND<170 Trichloroethene ND<170 <br />' 12-Dichlorobenzene ND<170 Tnchlorofluoromethane ND<170 <br /> 1,3 Dichlorobenzene ND<170 1,2,3-Trichloropropane ND<170 <br /> 1,4 Dichlorobenzene ND<170 1 2 4-Trime1hylbenzene 2200 <br /> Dichloroditluoromethane ND<170 1 3 5-Trimeth}lbenzene 610 <br />' 1 l Dichloroethane ND<170 Vin)I Acetate""' ND<170 <br /> 12-Dichloroethane ND<170 Vinyl Chloride"" ND<170 <br /> I 1-Dichloroethene ND<170 `C lenes,total '°' 9700 <br /> cis-I 2-Dichloroethene ND<170 <br />' trans-l2-Dichloroethene ND<170 <br /> i,2-Dichloropropane ND<170 <br /> 1,3-Dichloropropane ND<170 <br /> 2 2-Dichloropropane ND<170 Comments <br />' I,l-Dichloropropene ND<170 Surrogate Recokeries(%) <br /> cis-1,3-Dichloropropene ND<170 Dibromotluoromethane 94 <br /> trans-1,3-Dichloropropene ND<170 Toluene-d8 100 <br /> Ethylene dibromide ND<170 4-Bromotluorobenzene 105 <br />' Rater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, %apor samples 0 5 ug/L, solid and sludge samples 5 ug/kg wipes <br /> 0 2ughkipe ND means not detected above the reporting limit,NIA means anal}te not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone (c) (2-chloroethoxy) ethe.nne (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than --5 vol % <br /> sediment 0)sample diluted due to high organic content (k)peaks piesent in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimelh ylbenzenes <br />' DHS Certification No 1644 //Z Edward Hamilton,Lab Director <br />