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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCANIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Ihttp//wwwmccampbelleo E-mail main@mccampbell com <br /> Advanced GeoEnvironmentaI Client Project ID Larry's Auto Date Sampled 09/04/01 <br /> 837 Shaw Road Date Received 09/05/01 <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 09/06/01 <br />' Client P O Date Analyzed 09/06/01 <br /> Oxygenated:Volatile Organics By GUMS <br /> EPA method 8260 modifted <br />' Lab 1D 76888 76889 76890 76891 <br /> MW 1/ MW2/ MW3/ MW4/ Reporting Limit <br /> Client ID 090401 090401 090401 090401 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug1L <br /> Di-isopropyl Ether(DIPE) ND ND<5 0 ND ND<50 5 0 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND<5 0 ND ND<50<50 5 0 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND<5 0 1 2 130 50 1 0 <br /> lie <br /> tert-Amyl Methyl Ether(TAME) ND ND<5 0 ND ND<50 50 10 <br />' tert-Butanol ND ND<25 ND ND<250 25 50 <br />' Surrogate Recoveries(%) <br />' Dibromofluoromethane 107 101 107 108 <br /> Comments <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water imnuscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,(1)sample diluted due to <br /> high organic content <br />' DHS Certification No 1644 Edward Hamilton,Lab Director <br /> • <br /> 1 <br />