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I110 2nd Avenue South,##D7,Pacheco,CA 94553-55 60 <br /> McCANDBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htlpI/www.mccampbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 03/23/99 <br /> 4005 North Wilson Way Date Received 03/25/99 <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 03/30/99 <br /> Client P O Date Analyzed 03/30/99 <br />' Volatile Organics By GC/MS <br /> EPA method 82b0 <br /> Lab ID 05829 <br />' Client ID MW113-23-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone i ND<38 trans-l,3-Dichloropropene ND<38 <br />' Benzene 1600 Ethylene dibromide ND<38 <br /> Bromoberizene ND<38 Ethylbenzene 570 <br /> Bromochloromethane ND<38 Hexachlorobutadiene ND<38 <br /> Bromodichloromethane ND<38 lodomethane ND<38 <br />' Bromoforrn ND<38 Isopropylbenzene ND<38 <br /> Bromomethane ND<38 p-Isopropyl toluene ND<38 <br /> n-Butyl benzene ND<38 Methyl butyl ketone' ND<38 <br /> sec-Butyl benzene ND<38 Methylene Chlondet') ND<38 <br />' tert-Butyl benzene ND<38 Methyl ethyl ketone ND<38 <br /> Carbon Disulfide 51 Methyi isobutyl ketones ND<38 <br /> Carbon Tetrachloride ND<38 Methyi tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<38 Naphthalene 1100 <br /> Chloroethane ND<38 n-Propyl benzene 110 <br /> 2-Chloroethyl Vinyl Ether` ND<38 Styrene ' ND<38 <br /> Chloroform ND<38 1,1,1,2-Tetrachloroethane ND<38 <br />' Chloromethane ND<38 1,1,2,2-Tetrachloroethane ND<38 <br /> 2-Chlorotoluene ND<38 Tetrachloroethene ND<38 <br /> 4-Chlorotoluene ND<38 Toluene"1 360 <br /> Dibromochloromethane ND<38 1,2,3-Tnchl orobenzene ND<38 <br /> 1,2-Dibromo-3-chloropropane ND<38 1,2,4-Tnchlorobenzene ND<38 <br /> Dibromomethane ND<38 1,1,1-Trichloroethane ND<38 <br /> 1,2-Dichlorobenzene ND<38 1,1,2-Trichloroethane ND<38 <br /> 1,3-Dichlorobenzene ND<38 Trichloroethene ND<38 <br />' 1,4-Dichlorobenzene ND<38 Trichlorofluoromethane ND<38 <br /> Dichlorodifluoromethane ND<38 1,2,3-Tnchloropropane ND<38 <br /> l,l-Dichloroethane ND<38 1,2,4-Tnmethylbenzene 650 <br /> 1,2-Dichloroethane ND<38 1,3,5-Tnmethylbenzene 140 <br />' 1,1-Dichloroethene ND<38 Vinyl Acetate ° 110 <br /> cis-1,2-Dichloroethene ND<38 Vinyl Chloride ° ND<38 <br /> trans-l,2-Dichloroethene ND<38 Xylenes,total IN 1800 <br /> 1,2-Dichloropropane ND<38 Comments j <br />' 1,3-Dichloropropane ND<38 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<38 Dibromofluoromethane 94 <br /> LI-Dichloropropene ND<38 Toluene-d8 100 <br /> cis-1,3-Dichloropropene I ND<38 4-Bromofluorobenzene 92 <br />' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated .%ater samples I ug/l-,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/w1pe <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-but2none, (g) 4-methyl-2- <br /> pentanone or isopropylacetonc, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chlomethene,(o)dimethylbenzenes <br /> DHS Certif cation No 1644 � � Edward Hamilton, Lab Director <br />