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GeoAnalytical Laboratories , Inc . <br /> 2300 Maryann Dr. Turlock, CA 95380 Phone (209) 669-0100 Fax (209) 593 -2212 <br /> email : infoftcoanalyticallab,com <br /> Date : 12/09/ 19 <br /> Report # F9K1820 <br /> Date Recd : 11 / 18/ 19 <br /> Jim Thorpe, Inc . Project : 12667 Mundy Rd , Lodi CA <br /> P . O Box 357 <br /> Lodi , CA 95241 <br /> Volatile Organic Chemistry - Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD J <br /> Analvte Result Limit Units Level Result %REC Limits RPD Limit Notes J <br /> Batch F004175 - 8260B - EPA 5030 Prepared : 11 /21 /19 Analyzed : 12/04/19 - <br /> LCS (F004175-BS1 ) <br /> - ----- - --- --- . _ . . --- - -- -.__ -- - - - -. _ ._ _ 4444 . _ . <br /> I , 1 -Dichloroethane 63 .9 5 .0 ug/kg 60.00 107 80- 120 <br /> Benzene 65 . 1 5 .0 60. 00 109 80- 120 <br /> Methyl tert-Butyl Ether (MTBE) 62. 1 5 . 0 60. 00 104 80- 120 <br /> Monochlorobenzene 63 .3 5 .0 60. 00 105 80- 120 <br /> Toluene 64.5 5 .0 60.00 107 80- 120 <br /> Trichloroethylene 65 .0 5 . 0 60.00 108 WIN <br /> Surrogate: 1 , 2-Diehloroethane44 9. 68 10. 00 97 72432 <br /> Surrogate: 2-Bromo- l -Chloropropane 9. 76 10. 00 98 71434 <br /> Surrogate: 4-Bromofluoroben:ene 9. 88 10. 00 99 73432 <br /> Matrix Spike (F004175-MSI ) Source: F9K1820-01 <br /> l , l -Dichloroethane 58 .5 5 . 0 ug/kg 60 , 00 ND 98 73- 144 <br /> Benzene 55 . 5 5. 0 It 60.00 ND 92 64 . 8434 <br /> Methyl tert-Butyl Ether (MTBE) 72 .9 5.0 60.00 ND 122 75- 139 <br /> Monochlorobenzene 56.2 5 . 0 60 .00 ND 94 59- 151 <br /> Toluene 53 .2 5 .0 60.00 ND 89 67- 135 <br /> Trichloroethylene 59. 8 5 .0 60.00 ND 100 69443 <br /> - _ _4444- - -- - -. . . -- - -- --- - - . _ . . . - -- - - - -- -. _.. _. . ----- -- . . - -- --- - -- -- - -- - - - <br /> Surrogate: 1 , 2-Dichloroethane-d4 13. 7 10. 00 137 72432 S-GC <br /> Surrogate: 2-Bramo- l -Chloropropane 10. 2 1000 102 71434 <br /> Surrogate: 4-Bromofluorobenzene 11 . 0 10. 00 110 74431 <br /> Matrix Spike Dup (F004175-MSDI ) Source: F9K1820-01 <br /> . _ . . _. . ._ - - <br /> 1 , l -Dichloroethane 58 .6 5 .0 ug/kg 60 .00 ND 98 73- 144 0.2 18 <br /> Benzene 55 .3 5 .0 60 .00 ND 92 64. 8- 134 0.3 16 <br /> Methyl tert-Butyl Ether (MTBE) 7342 5 .0 60.00 ND 122 75- 139 0. 3 20 <br /> Monochlorobenzene 57 . 1 5 .0 60.00 ND 95 59- 151 2 19 <br /> Toluene 54 , 1 5 .0 60. 00 ND 90 67 - 135 2 13 <br /> Trichloroethylene 6041 5 .0 60.00 ND 100 69- 143 0 . 6 15 <br /> - - -- -- -- --- - 444 _ 4 . -- --- - -. - ----- -- <br /> Surrogate: 1 , 2-Dichloroethane-d4 13. 8 10. 00 138 72431 S-GC <br /> Surrogate: 2-Bromo- l -Chloropropane 10. 2 10. 00 / 01 7 /434 <br /> Surrogate: 4-Bromofluoroben:ene 1/ . ! 10. 00 H / 74- 132 <br /> E <br /> Certification # 2585 <br /> k <br /> l <br />