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RECEIVED <br /> MAR 1 1 2019 <br /> Excelchem Laboratories , Inc . <br /> P11111 : 1 S11111 �� I <br /> Sol <br /> ISO NEW III III III III III III I SEE III III <br /> Project: <br /> A&A Transmission PERMIPSERVICES <br /> =RiverRd. <br /> Date Reported: <br /> Project Number: [none] <br /> David Hendricks 01 /28/ 19 09 :04 Project Manager: <br /> Total Recoverable Metals - Quality Control <br /> 11 SEE III SEE IIII Sol IIII <br /> Me Me MEN III Me <br /> Spike Source %REC �'D <br /> Rel t b Units Level Result %REC Limits RPD Limit Notes <br /> Result <br /> Analyte <br /> IIII SEE SEE <br /> Batch A A0165 - EPA 6010BNEW <br /> Source : 1901100-01 Prepared: 01 /21 / 19 Analyzed: 01 /22/ 19 --- <br /> Matrix Spike (A]A0165-MSI ) _ - - - - - - - QM-01 <br /> - - 63 .0 - - Lo mg/kg 100 IO.G 52.5 75- 125 <br /> Antimony 10 100 1 . 13 98.0 75- 125 <br /> Arsenic 99. 1 <br /> 328 <br /> 2.0 to 100 251 77.3 75- 125 <br /> Barium 0.5 „ 100 ND 96.3 75- 125 <br /> Beryllium 11 96.3 <br /> 1 .0 100 14.8 94.8 75- 125 <br /> Cadmium 169 1 .0 100 78 .0 88.8 75- 125 <br /> Chromium 100 6. 15 91 .4 75- 125 <br /> 97 .5 5 .0 <br /> Cobalt 100 1070 2.00 75- 125 QM-() 1 <br /> Copper Co 1070 2.0 QM -01 <br /> p 1 .0 100 644 226 75- 125 Q <br /> Lead 870 <br /> 205 1 .0 100 127 79 .0 75- 125 <br /> Molybdenum 164 1 .0 100 82,4 81 . 1 75- 125 <br /> Nickel 89.6 2.0 loo ND 89.6 75- 125 <br /> Selenium 87 .5 1 .0 loo ND 87.5 75- 125 <br /> Silver 82.5 2.0 100 0.960 81 .5 75425 <br /> Thallium 9G.2 2.0 too 4,05 92. 1 75- 125 <br /> Vanadium 2.0 100 1030 NR 75- 125 E , QM -UI <br /> Zinc 1020 <br /> Matrix Spike Dup (AJA0165-MSD1 ) <br /> Source: 1901100-01 Prepared: 0 1 /21 / 19 Analyzed: 01 /22/ 19 _ - <br /> - - - - - _ -- 65 .9 -- - 1 .0 mg/kg 100 10.6 55.3 75- 125 4.44 25 <br /> Antimony 10 100 1913 100 75- 125 2.29 25 <br /> Arsenic 101 100 251 93 .4 75- 125 4.79 25 <br /> 2,0 <br /> Barium 344 9R . 1 0.5 of 100 ND 98 . 1 75- 125 1 .88 25 <br /> Beryllium 1 . 0 It too 14 .8 98.5 75- 125 3 .32 25 <br /> Cadmium 1 l3 <br /> 177 1 .0 IOU 78.0 98.7 75- 125 5.77 25 <br /> Chromium I0U 5 . 0 100 6. 15 93 .8 75425 2 .52 25 Cobalt 100 1070 114 75- 125 9.95 <br /> 25 <br /> 1180 2 .0 <br /> Copper ISO too 644 108 75- 125 14.6 25 <br /> Lead 752 <br /> 229 1 .0 100 127 102 75- 125 11 .2 25 <br /> Molybdenum 179 L0 100 82,4 96.5 75- 125 9.00 25 <br /> Nickel 91 .4 2.0 100 ND 91 .4 75- 125 1 .98 25 <br /> Selenium 100 ND 89.5 75- 125 2.21 25 <br /> 89.5 I .0 <br /> Silver 84.8 2.0 98.2 2.0 it 100 0.960 83 .8 75- 125 2.74 25 <br /> Thallium 100 4.05 94. 1 75- 125 2 .06 25 <br /> Vanadium 100 1030 81 .0 75- 125 8.72 25 <br /> E <br /> IIIU 2.0 <br /> Zinc <br /> III Me I <br /> The results in this repa't aPI to the samples am()zed in accordance with the chain of <br /> Excelchem Environmental Labe custody, document. This analytical report must be reproduced in its entirety. <br /> c <br /> i <br /> \ Page 6 of 7 <br /> Laboratory Representative <br />