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9 <br /> PAHs using EPA Method 8310; TPH as gasoline, diesel and motor oil using EPA Method 8015; <br /> and for Title 22 Metals using the EPA Method 6010/7000 Series. <br /> 4.4.2 Soil Gas Sampling <br /> Volatile organic compound impacts identified in Soil Gas Sample A3-SG1 will be delineated <br /> through the installation and sampling of proposed Soil Gas Borings A3-SG2 through A3-SG6. <br /> Sampling will be conducted in the warehouse area adjacent to the existing office building and <br /> adjacent to the northern boundary of the Site near the electrical substation. The data generated <br /> through the installation and sampling of these soil gas borings will assist with the <br /> characterization of the Site and the provide information that will assist in the determination of <br /> the potential for vapor intrusion into the on-site buildings. Additionally, PCE impacts identified <br /> in Soil Gas Boring Al-SGI will be delineated with the installation of Soil Gas Borings Al-SG2 <br /> and Al-SG3, located northeast and southwest of Al-SGI, respectively. These soil gas points <br /> will assist in the determination of PCE impacts and their potential source. <br /> All soil gas samples will be analyzed using EPA Method TO-15 and will include naphthalene. A <br /> real-time leak test will be performed at each probe location using either helium or a duster as a <br /> tracer compound. The tracer compound will be placed around the probe seal at the surface <br /> utilizing a shroud to encompass the sampling train. A sample will then be drawn from the <br /> probeltubing into a new Tedlar bag and tested for the tracer compound with a hand-held detector <br /> to ensure that ambient air does not dilute or contaminate the soil gas sample. If leakage is <br /> confirmed(>10% of the concentration introduced into the shroud), the source of the leak will be <br /> identified, repaired and the real-time leak check will be conducted again. This will continue <br /> until all leaks have been repaired; thus allowing the collection of the soil gas sample. The <br /> following real-time leak check protocols for helium and/or the duster compound have been <br /> developed for this Site based on the January 30, 2009 letter from DTSC to PG&E, referencing <br /> new leak detection procedures. <br /> Soil Gas Ambient Air Leak Detection Protocol using Helium <br /> Real-time leak testing procedures using helium as the tracer compound will be accomplished as <br /> follows: <br /> 1. Introduce the tracer gas around the sample probe and canister by filling a shroud <br /> (such as a plastic bucket)positioned over the sample location. <br /> 2. Make sure the shroud is suitably sealed to the ground surface. <br /> 3. Introduce the tracer gas into the shroud. Helium should be injected into the shroud at <br /> 5 psi. The shroud will have tubing at the top of the chamber to introduce the tracer <br /> gas into the shroud and a valve fitting at the bottom to let the ambient air out while <br /> introducing tracer gas. The helium concentration within the shroud will be monitored <br /> with a field helium detector and maintained at 30%. <br /> 4. The shroud will have a gas-tight fitting or sealable penetration to allow the soil vapor <br /> sample probe tubing to pass through and exit the chamber. <br /> 5. Attach the sample probe tubing exiting the shroud to a pump that will be pre- <br /> calibrated to extract soil vapor at a rate of no more than 0.2 liters per minute. <br />