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LancasterAnalysis Report` <br /> Laboratories Y • <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605.2425*717-6562300 Fax 717-656-2681 www IancasterlabS com <br /> Page 4 of 4 <br /> Quality Control SuimYtary <br /> Client Name ChevronTexaco Group Number 965812 <br /> Reported 11/15/05 at 11 25 AM <br /> Surrogate Quality Control <br /> Limits 59-131 <br /> Analysis Name BTEX+MTBE by B260E <br /> Batch number Z0530B2AA <br /> Dibromo€luoromethane 1,2-Dichloroethane-d4 Toluene-dB 4-Bromofluorobenzene <br /> 4638628 94 97 43 S9 <br /> 4638629 96 96 93 89 <br /> 4638630 94 96 94 91 <br /> 4638631 92 93 93 90 <br /> 4638632 91 90 93 89 <br /> 4638637 92 90 92 88 <br /> Blank 89 87 93 86 <br /> LCS 88 87 93 89 <br /> MS 89 89 94 90 <br /> MSD 91 89 94 89 <br /> Limits BO-116 77-113 80-113 76-113 <br /> Analysis Name BTEX+5 dxygenates+EDC+EDB+ETOH <br /> Batch number Z053113AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-dB 4-Bromofluorobenzene <br /> 4638633 BB 78 87 63 . <br /> 4638634 89 79 87 83 <br /> 4638635 Be 79 87 84 <br /> 4638636 89 76 87 64 <br /> Blank Be 80 86 63 <br /> LCS 88 78 87 85 <br /> MS Be 78 86 84 <br /> MSD 88 78 87 85 <br /> Limits 80-116 77-113 F 80-113 78-113 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added • <br />