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Lancaster <br /> Laboratories analysis Report <br /> 2425 New Holland Pike,PO Box 12425 Lancaster,PA 17605-2425•717-656 2300 Fax 717-656-2681•www lancasterlabs com <br /> Page 2 of 5 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 873162 <br /> Reported 11/14/03 at 09 31 AM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result FIDL Units !kREC REC Limits RPD RPD Max <br /> Sample Matrix Quality Control <br /> MS MSD MS/MSD RPD BKG DUP DDP Dup <br /> RPD <br /> Analysis Name REC %REC Limits RPD MAX cont Conc RPD Max <br /> Batch number 033080009A Sample number(s) 4155520-4155522 <br /> Methanol (by Direct Injection) 104 104 73-117 0 20 <br /> Batch number 033080011A Sample number(s) 4155523 <br /> Methanol (by Direct In)ection) 104 108 73-117 4 20 <br /> Batch number 03308112601A Sample number(s) 4155524 <br /> TRPH 418 1 0 42 1 5 113* (1) 34 <br /> Batch number 03309A07B Sample number(s) 4155515-4155519 <br /> TPH-GRO - Waters 100 104 63-154 2 30 <br /> Batch number 03309A07C Sample number(s) 4155520-4155524 <br /> TPH-GRO - Waters 100 104 63-154 2 30 <br /> Batch number P033072AA Sample number(s) 4155515-4155516 <br /> Methyl Tertiary Butyl Ether 100 102 69-134 2 30 <br /> Benzene 110 112 83-128 1 30 <br /> Toluene 113 113 83-127 0 30 <br /> Ethylbenzene 112 113 82-129 0 30 <br /> Xylene (Total) 115 114 82-130 1 30 <br /> Batch number P033092AA Sample number(s) 4155517-4155519 <br /> Methyl Tertiary Butyl Ether 96 101 69-134 3 30 <br /> Benzene 116 88 83-128 17 30 <br /> Toluene 110 109 83-127 1 30 <br /> Ethylbenzene 110 109 82-129 1 30 <br /> Xylene (Total) 109 109 82-130 1 30 <br /> Batch number P033102AA Sample number(s) 4155524 <br /> Methyl Tertiary Butyl Ether 101 101 69-134 0 30 <br /> Benzene 110 110 83-128 1 30 <br /> Toluene 110 111 83-127 2 30 <br /> Ethylbenzene 111 112 82-129 2 30 <br /> Xylene (Total) 110 112 82-130 2 30 <br /> Batch number P033113AA Sample number(s) 4155520-4155523 <br /> Ethanol 99 98 38-149 1 30 <br /> Methyl Tertiary Butyl Ether 97 97 69-134 0 30 <br /> di-Isopropyl ether 94 95 75-130 1 30 <br /> Ethyl t-butyl ether 91 92 78-119 1 30 <br /> t-Amyl methyl ether 99 99 77-117 1 30 <br /> t-Butyl alcohol 103 95 44-150 7 30 <br /> Benzene 97 92 83-128 2 30 <br /> 1,2-Dlchlaroethane 95 95 73-136 1 30 <br /> Toluene 103 103 83-127 1 30 <br /> 1,2-Dibromoethane 94 95 78-120 0 30 <br /> Ethylbenzene 103 99 82-129 2 30 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />