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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 1900 Bates Avenue,Suite L Concord,CA 94520 (510) 686 9600 FAX(510) 686 9689 <br /> qWr Analytical 819 Striker Avenue Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX (916) 921 0100 <br /> OMPDS Services Client project ID Unocal #6981, 4707 Pacific Ave , Stockton <br /> 2401 Stanwell Dr , Ste 400 Matrix Liquid <br /> Concord, CA 94520 <br /> Attention Avo Avedlssian QC Sample Group 5011287-299 Reported Feb 10, 1995 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Benzene Toluene Ethyl Xylenes <br /> Benzene <br /> Method EPA 8020 EPA 8020 EPA 8020 EPA 8020 <br /> Analyst M Creusere M Creusere M Creusere M Creusere <br /> MS/MSD <br /> Batch# 5011295 5011295 5011295 5011295 <br /> Date Prepared 2/2/95 2/2/95 2/2/95 2/2/95 <br /> Date Analyzed 2/2/95 2/2/95 2/2/95 2/2/95 <br /> Instrument I D # HP-2 HP-2 HP-2 HP-2 <br /> Conc Spiked- 20lig/L 20Yg/L 20pg/L 60lig/L <br /> Matrix Spike <br /> % Recovery 90 100 105 108 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery 85 100 105 105 <br /> Relative % <br /> Difference 57 0 0 00 2 8 <br /> LCS Batch# 1 LCS020295 1 LCS020295 1 LCS020295 1 LCS020295 <br /> Date Prepared 2/2/95 2/2/95 2/2/95 2/2/95 <br /> Date Analyzed 2/2/95 2/2/95 2/2/95 2/2/95 <br /> Instrument 1 D # HP-2 HP 2 HP-2 HP-2 <br /> LCS % <br /> Recovery 88 104 112 114 <br /> % Recovery <br /> Control Limits 71-133 72-128 72-130 71-120 <br /> Please Note <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> SEQUOIA ANALYTICAL, #1271 preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> .Signature on File the recovery of analytes from the matrix spike does not fall within specrfied control limits due to matrix <br /> Interference,the LCS recovery is to be used to validate the batch <br /> Alan B Kemp <br /> Project Manager <br /> 5011287 MPD <5> <br /> fid' <br />