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r Sequoia 680 Chesapeake Dnve Redwood Gry, CA 94063 (415) 364 9600 FAX (415) 364 9233 <br /> 404 N W�get Lane Walnut Creek CA 94598 (510) 988 9600 FAX (510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento, CA 95834 (916) 921 9600 FAX (916)921 0100 <br />*MPDS Services Client Project ID Unocal #6981, 4707 Pacific Ave , Stockton <br /> 2401 Stanwell Dr, Ste 300 Matrix Liquid <br /> Concord, CA 94520 <br /> Attention Sarkis Karkarian OC Sample Group 5072006-18 Reported Aug 10, 1995 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Benzene Toluene Ethyl Xylenes <br /> Benzene <br /> Method EPA 8020 EPA 8020 EPA 8020 EPA 8020 <br /> Analyst J Fontecha J Fontecha J Fontecha J Fontecha <br /> MS/MSD <br /> Batch# 5072001 5072001 5072001 5072001 <br /> Date Prepared 8/6/95 8/6/95 8/6/95 8/6/95 <br /> Date Analyzed 8/6/95 8/6/95 8/6/95 8/6/95 <br /> Instrument I D # HP-9 HP-9 HP-9 HP-9 <br /> Conc Spiked 20 ug/L 20 yg/L 20 ug/L 60 ug/L <br /> Matrix Spike <br /> % Recovery 110 115 115 123 <br /> Matrix Spike <br /> Duplicate % <br /> Recovery 110 115 115 128 <br /> Relative% <br /> Difference 00 00 00 40 <br /> LIDS Batch# 4LCS080695 4LCS080695 4LCS080695 4LCS080695 <br /> Date Prepared 8/6/95 8/6/95 8/6/95 8/6/95 <br /> Date Analyzed 8/6/95 8/6/95 8/6/95 8/6/95 <br /> Instrument I D # HP-9 HP 9 HP-9 HP-9 <br /> LCS % <br /> Recovery 95 99 97 106 <br /> Recovery <br /> Control Limits 71-133 72-128 72-130 71-120 <br /> Please Note <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> SEQUOIA ANALYTICAL, #1271 preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> aignature on File the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> Alan B Kemp interference,the LCS recovery is to be used to validate the batch <br /> Project Manager <br /> Q 5072006 MPD <5> <br />