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oad <br /> Sequoia los. Industrial 1II <br /> San Carlos.CA 94070-411 1 <br /> (650)7.32-9600 <br /> Analytical �uotalabs <br /> ' <br /> 0 <br /> Gettler-Ryan/Gcostratep*l) Project. Tosco(5) Sampled. 6126/00 <br /> 6747 Sierra Court,Suite j Project Number Tosco(Unocal)SS#6981 Rooerved. 6/27100 <br /> Dabluu;CA 94568 = -- _ ---- Project Manager Deanna Harding--- - Reported-7/12100- - <br /> Date Spike Sample QC Reporting Limit Remy RPD RPD <br /> Anal Analyzed Level Result Result Umts Recov Limits % Limit % Notes' <br /> Batch 0070014 pate Prepared. 715100 Extraction Method: EPA 5030B FPM <br /> Blank 0070014-BLKI <br /> Ethanol 7/5100 ND ug/l 1000 <br /> Tert-butyl alcohol ^ ND " 100 <br /> Methyl tent butyl ether ND " 2.00 <br /> Di-isopropyl ether ND " 2.00 <br /> Ethyl tert-butyl ether ND 200 <br /> Teat-amyl methyl ether ND " 2.00 _ <br /> Surrogate. 1,2 Drchloroethane-d4 IV Soo 519 760-114 104 <br /> Blank 0070014-BLK2 <br /> Ethanol 7/6/00 ND ug/1 1000 <br /> Tert-butyl alcohol ND 100 <br /> Methyl tert-butyl ether ND " 2.00 <br /> Di-isopropyl ether M ND " 2.00 <br /> Ethyl tart-butyl ether ND 200 <br /> Text-amyl methyl ether " ND 2.00 <br /> Surrogate. 42 Drchloroethane-d4 " Soo 527 " 760-114 105 <br /> LCS 0070014-BS1 <br /> Methyl text-butyl ether _ 715100 Soo 413 ug/I 700-130 826 <br /> Surrogate 1,2 Drchloroethane-d4 or 500 522 " 760-114 104 <br /> LCS 0070014-BSg <br /> Methyl tent butyl ether 7/6/00 500 365 ug/l 700-130 73 0 <br /> Surrogate 1,2 Drchloroethane-d4 Ff 500 526 " 760-114 105 <br /> Ma ��1 -17t007004 <br /> Methyl tertbutyl ether 7/5/00 Soo ND 40 2 ug/l 600-140 _80.4 <br /> Surrogate. 1,24hchlomethane-d4 ^ 500 528 ff 760-114 106 <br /> Matrix Svike D 0 0070014-MSD1 L006210-17 <br /> Meth i teat-butyl ether 715100 50 0 ND 40 2 ug/L 60 0-140 80A 250 0 <br /> Surrogate 1,2-Drchlor�oethane-d4 SO 0 S3 8 76 0-114 108 <br /> Batch 0072Q23 Date Pre red- 7/6100 Extraction Method: EPA 5030B IFM <br /> Blank 007002 -B GKI <br /> Ethanol 7/6/00 ND ug/l 1000 <br /> Tert-butyl alcohol ND 100 <br /> Methyl tert-butyl ether ND 2.00 <br /> Ek-isopropyl ether ND 2.00 <br /> Ethyl tat butyl ether - ^——... ND " 2.00 <br /> Sequoia Analytical-San Carlos *Refer to end of roport for text of notes and defin1doa <br /> Page 27 of 30 <br />