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I / <br /> ! 819 Striker Avenue Suite 8 <br /> Sego�Ya Sacramento CA 95834 <br /> ® (916) 921-9600 <br /> FAX(916) 9Z 1-0 100 <br /> Analytical www secluoialab5 com <br /> Gettler-Ryan-Petaluma Project Former Tosco 6981, Stockton,CA 5208311 <br /> 1364 N McDowell Blvd Ste B2 Project Number NIA Reported <br /> Petaluma CA,94954 Project Manager Dave Vossler 08/29/02 14 28 <br /> GasolinelBTEXIOxygenates by EPA method 8260B - Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> Malyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 2080283-EPA 5030B JP/TJ <br /> Matrix Spike(2080283-MSI) Source 5208359-08 Prepared&Analyzed 08/28/02 <br /> Benzene 144 050 ug/l 134 ND 107 70-130 <br /> Toluene 804 0 50 81 0 ND 99 70-130 <br /> Methyl tent-butyl ether 279 050 21 8 55 103 60-140 <br /> Gasoline(c6-CIO) 1010 50 1100 ND 92 60-140 <br /> Surrogate 12-DCA-d4 211 250 84 60-140 <br /> Surrogate Toluene d8 233 250 93 60-140 <br /> Surrogate 4-BFB 238 250 95 60-140 <br /> Matrix Spike Dup(2080283-MSD1) Source 5208359-08 Prepared&Analyzed 08/28/02 <br /> Benzene 144 050 ug/I 134 ND 107 70-130 0 25 <br /> Toluene 81 4 050 81 0 ND 100 70-130 1 25 <br /> Methyl tert butyl ether 286 050 21 8 5 5 106 60-140 2 25 <br /> Gasoline(C6-Cl0) 988 50 1100 ND 90 60-140 2 25 <br /> Surrogate 1 2-DCA-d4 207 250 83 60-140 <br /> Surrogate Toluene d8 238 250 95 60-140 <br /> Surrogate 4-BFB 238 25 0 95 60-140 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the than <br /> custody document This analytical report must be reproduced in its entirety <br /> Page 6 of 7 <br />