Laserfiche WebLink
V <br /> 1.1 <br /> GROUN12WATER SAMPLE COLLECTION <br /> This section describes the routine procedures followed by HETI while collecting groundwater <br /> samples for chemical analysis. These procedures include decontamination, water level <br /> measurements, well purging, physical parameter measurements, sample collection, sample <br /> preservation,and sample handling. Critical sampling objectives for HETI are to: <br /> 1. Collect groundwater samples which are representative of the sampled matrix. <br /> 2. Maintain sample integrity from the time of sample collection to delivery to the analytical <br /> laboratory. <br /> Sample analyses, methods, containers, preservation, and holding times are presented in Table <br /> A-1. <br /> V <br /> rr All physical parameter measuring and sampling equipment shall be decontaminated prior to <br /> measurement and sample collection using a trisodium phosphate or Alconox solution wash, <br /> followed by two separate rinses in tap water, followed by one rinse in steam-distilled water. <br /> Any sampling equipment surfaces or parts that might absorb specific contaminants, such as <br /> plastic pump valves,impellers,etc.,are to be cleaned in the same manner. <br /> Sample bottles,bottle caps, and septa used for sampling volatile organics are thoroughly pre- <br /> cleaned in either the laboratory or the factory. All appropriate measures shall be taken to <br /> assure continued sterility of the containers issued by the contract laboratory prior to usage at <br /> the project site. <br /> y During field sampling, equipment which has been placed in a well shall be decontaminated by <br /> washing with a trisodium-phosphate or Alconox solution followed by two rinses in tap water <br /> and one rinse in steam-distilled water. <br /> Water Level Measurements <br /> �. Prior to purging and sampling any wells, the static-water level shall be measured by use of an <br /> electronic sounder and/or calibrated portable oil-water interface probe. Both static water <br /> level and separate phase product thickness shall be measured and noted to the nearest ±0.01 <br /> �. foot. Interface probe results shall be confirmed by sampling the top of the water column with a <br /> clear bailer and measuring any floating product thickness to the nearest ±0.01 foot with an <br /> engineers scale tape. In all cases a clear bailer sample will be taken from each well to check for <br /> color,sheen and undetected floating product. If floating product of any measureable thickness is <br /> `r observed, no sampling will be performed for that well. If visible product sheen is observed, <br /> sampling shall proceed under normal protocols. <br /> �.. The line used to lower the bailer shall be discarded after each use to preclude the possibility of <br /> cross contamination. Field observations (e.g., well integrity, product odor, turbidity, water <br /> color, odors, etc.) shall be recorded on the HETI Purge/Sample Sheet (Plate A-2). Before and <br /> after the use of the electric sounder, interface probe, non-dedicated bailer, or any other down <br /> well equipment, each will be decontaminated by washing in a trisodium phosphate or Alconox <br /> solution, followed by a double rinse with tap water, followed by a rinse with steam-distilled <br /> water. <br /> v <br /> V <br /> 9 <br /> 6" <br />