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L ' <br /> - �-] I F,JEJLA Ir <br /> L CORE LABORATORIES <br /> k <br /> Q UAL I T Y C 0 N T R 0 L R E S U L T S <br /> Job Number: 981628{ Date: 10/29/98 r� <br /> CUSTOM(R Fluor Dan�e.l GT[ PROJECT SL 20304/1D2480 <br /> hTTN Shelby Lathrop <br /> QC Type Description Re 9. Code Lab ID Dilution Factor Date <br /> Time <br /> Test Method........: EPA 8260E <br /> Batch........: 3392 Analyst gfb <br /> Method Description.: Volatile organics by GC/MS Units........: ug/L <br /> I <br /> f <br /> MB Method Blank <br /> 1:0/26/9$:: 1647 <br /> Parameter/Test Description QC Result QC Result True Value Orig. Value Calc. Result * Limits <br /> Ui-yl <br /> t-Butyl Alcohol (TBA) -74.45 100 <br /> Isopropyl Ether _2.96 L <br /> tert-Butyl Ether (ETBE) 5.00 <br /> 1-40 <br /> tent-Amyl Methyl Ether -0.86 5.005.00 <br /> ethyl-t-Butyl Ether (MTBE) -7.56 30.00 <br /> I <br /> M.S Matrtx spike 08092701 981627 1< 1000:: <br /> Parameter/Test Description QC Result QC Result True Value Orig. Value Calc. Result * Limits <br /> TBA Alcohol <br /> 4ert-Butyl { } 537.64 500.000000 0 107.5 % 75-125 <br /> Di-Isopropyl Ether 25.20 25.000000 -3.27 113.9 % 75-125 <br /> -thy[ tert-Butyl Ether (ETBE) 26.88 25.000000 0 107.5 % 75-125 <br /> ert-Amyl Methyl Ether 28.64 25.000000 0 114.6 % 75-125 <br /> ethyl-t-Butyl Ether (MTBE) 47.31 50.000000 -6.52 111.7 % 75-125 <br /> f I <br /> MSD Matrix Spike OupLIcate 08092301 981627 000 <br /> 1 : 1 : 10/27/98 0042 i <br /> Parameter/Test Description QC Result ult QC Result True value Orig. Value Calc. Result * Limits � <br /> i <br /> L-1sopropyl <br /> rt-Butyl Alcohol (TBA) 604.61 537.64 500.000000 0 120.9 % 75-125 <br /> 12 R 20 <br /> Ether 26.85 25.20 25.000000 -3.27 120.5 % 75-125 <br /> 6 R 20 F <br /> Ethyl tert-Butyl Ether (ETBE) 28.65 26.88 25.000000 0 114.6 % 75-125 <br /> 6 R 20 <br /> L rt-Amyt Methyl Ether 30.97 28.64 25.000000 0 123.9 % 75-125 <br /> 8 R 20 <br /> Methyl-t-Butyl Ether (MTBE) 51.39 47.31 50.000000 -8.52 119.8 1 75-125 <br /> 8 R 20 <br /> CCV conttnuin9':Caltbration Ve n facation 08092101 1000 3p%26/98 ",1617'::: <br /> .'r <br /> Parameter/Test Description QC Result QC Result True Value Orig. Value Calc, Result ' Limits <br /> rt-Butyl Alcohol (TBA) 399.05 <br /> 500.00DO00 80 % 80-120 Y <br /> Di-isopropyl Ether 22.51 25.000000 90 % 80-120 F <br /> hyl tert-Butyt Ether (ETBE) 22.89 25.000000 92 % 80-120 I <br /> rt-Amyl Methy{ Ether 23.46 25.000000 94 % 80-120 <br /> thy(-t-Butyl Ether (MTBE) 44.31 50.000000 89 % 80-120 f <br /> L k <br /> I <br /> i <br /> Page S <br /> REC R-RPD A-ABS Diff. D-% Diff. F <br /> .r;v.!,f•.•:;r.::n:. ...:..:::.:1, ,..q n1(:;;;.Ltlx,r.;,:w;...C,•n L.,,.n'n n.... ,rs r <br /> -".'i.•:.1 <br /> ........ <br /> �T <br /> - � J <br />