i
<br /> HLAB
<br /> CORE LABORATORIES
<br /> Q U A L I T Y A S S U R A N C E F 0 0 T E R
<br /> METHOD REFERENCES
<br /> (1) EPA Su-846, Test Methods for Evaluating Solid waste, Third Edition, September 1986, and Updates I, II, IIA, IIB, and III
<br /> (2) Standard Methods for the Examination of Slater and Wastewater, 18th Edition, 1992
<br /> (3) EPA 600/4-79-020, Methods of Chemical Analysis for Waters and Wastes, March 1983
<br /> (4) Federal Register, Friday, October 26, 1984 (40 CFR Part 136)
<br /> (5) American Society for Testing and Materials, Volumes 5.01, 5.02, 5.03, 1992
<br /> (6) EPA 600/4-89-001, Short-term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Fresh
<br /> Yater Organisms
<br /> (7) EPA 600/4-90-027, Methods for Measuring the Acute Toxicity of Effluent and Receiving Waters to Fresh Water and Marine
<br /> € Organisms, Fourth Edition
<br /> COMMENTS
<br /> { All methods of chemical analysis have a statistical uncertainty associated with the results. Unless otherwise indicated,
<br /> # the data in this report are within the limits of uncertainty as specified in the referenced method. Quality control
<br /> acceptance criteria are based either on Limits specified in the referenced method or on actual laboratory performance.
<br /> The date and time of analysis indicated on the QC report may not reflect the actual time of analysis for QC samples. Data
<br /> i reported in the QA report may be lower than sample data due to dilution of samples into the calibration range of the analysis.
<br /> Sample concentrations for solid samples are calculated on an as received (wet) basis unless otherwise indicated. Unless
<br /> otherwise indicated, volatiles by gas chromatography (GC) are reported from a single column. Volatiles analyses by GC on Low
<br /> level soils are conducted at room temperature. TCLP extractions are performed at sample amounts, approved by the State of
<br /> California.
<br /> FLAGS, FOOTNOTES, AND ABBREVIATIONS (as needed) f
<br /> NA = Not analyzed H.I. = Not Ignitable
<br /> N/A = Not applicable S.I, = Sustains Ignition F
<br /> ug/L = Micrograms per liter I(NS) = Ignites, but does not Sustain Ignition
<br /> mg/L = Milligrams per liter RPD = Relative Percent Difference
<br /> ND = Not detected at a value greater than the reporting Limit
<br /> HC = Not calculable due to values Lower than the detection Limit
<br /> (a) = Surrogate recoveries were outside acceptable ranges due to matrix effects.
<br /> (b) = Surrogate recoveries were not calculated due to diLution of the sample below the detectable range for the surrogate.
<br /> (c) = Matrix spike recoveries were outside acceptable ranges due to matrix effects.
<br /> (d) = Relative Percent Difference (RPD) for duplicate analysis outside acceptance limits due to actual differences in
<br /> }, the sample matrix.
<br /> (e) = The Limit listed for flammability indicates the upper Limit for the test. Samples are not tested at temperatures
<br /> above 140 Fahrenheit since only samples which will sustain ignition at temperatures below 140 are considered
<br /> 9 �
<br /> flammable.
<br /> (f) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern. Results were quantified using a
<br /> diesel standard, however, the hydrocarbon pattern did not match a diesel pattern_
<br /> i (g) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern. Results were quantified using a
<br /> gasoline standard, however, the hydrocarbon pattern did not match a gasoline pattern.
<br /> (h) = High dilution due to matrix effects
<br /> QC SAMPLE IDENTIFICATIONS SUBCONTRACTED LABORATORY LOCATIONS
<br /> MB = Method Blank SB = Storage Blank Core Laboratories: Aurora, Colorado *AU
<br /> RB = Reagent Blank MS = Matrix Spike Casper, Wyoming *CA
<br /> ICB = Initial Calibration Blank MSD = Matrix Spike Duplicate Corpus Christi, Texas *CC
<br /> CCS = Continuing Calibration Blank MD = Matrix Duplicate Edison, New Jersey *ED
<br /> CS = Calibration Standard SS = Blank Spike Houston, Texas (Env) *HE
<br /> ICV = Initial Calibration SS = Surrogate Spike Houston, Texas (Pet) *HP
<br /> Verification LCS = Laboratory Control Indianapolis, Indiana *IN
<br /> CCV = Continuing Calibration Standard Lake Charles, Louisiana *tC
<br /> Verification RS = Reference Standard Long Beach, California *L9
<br /> Valparaiso, Indiana *VP
<br /> Bakersfield, California *BK
<br /> i
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