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i <br /> HLAB <br /> CORE LABORATORIES <br /> Q U A L I T Y A S S U R A N C E F 0 0 T E R <br /> METHOD REFERENCES <br /> (1) EPA Su-846, Test Methods for Evaluating Solid waste, Third Edition, September 1986, and Updates I, II, IIA, IIB, and III <br /> (2) Standard Methods for the Examination of Slater and Wastewater, 18th Edition, 1992 <br /> (3) EPA 600/4-79-020, Methods of Chemical Analysis for Waters and Wastes, March 1983 <br /> (4) Federal Register, Friday, October 26, 1984 (40 CFR Part 136) <br /> (5) American Society for Testing and Materials, Volumes 5.01, 5.02, 5.03, 1992 <br /> (6) EPA 600/4-89-001, Short-term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Fresh <br /> Yater Organisms <br /> (7) EPA 600/4-90-027, Methods for Measuring the Acute Toxicity of Effluent and Receiving Waters to Fresh Water and Marine <br /> € Organisms, Fourth Edition <br /> COMMENTS <br /> { All methods of chemical analysis have a statistical uncertainty associated with the results. Unless otherwise indicated, <br /> # the data in this report are within the limits of uncertainty as specified in the referenced method. Quality control <br /> acceptance criteria are based either on Limits specified in the referenced method or on actual laboratory performance. <br /> The date and time of analysis indicated on the QC report may not reflect the actual time of analysis for QC samples. Data <br /> i reported in the QA report may be lower than sample data due to dilution of samples into the calibration range of the analysis. <br /> Sample concentrations for solid samples are calculated on an as received (wet) basis unless otherwise indicated. Unless <br /> otherwise indicated, volatiles by gas chromatography (GC) are reported from a single column. Volatiles analyses by GC on Low <br /> level soils are conducted at room temperature. TCLP extractions are performed at sample amounts, approved by the State of <br /> California. <br /> FLAGS, FOOTNOTES, AND ABBREVIATIONS (as needed) f <br /> NA = Not analyzed H.I. = Not Ignitable <br /> N/A = Not applicable S.I, = Sustains Ignition F <br /> ug/L = Micrograms per liter I(NS) = Ignites, but does not Sustain Ignition <br /> mg/L = Milligrams per liter RPD = Relative Percent Difference <br /> ND = Not detected at a value greater than the reporting Limit <br /> HC = Not calculable due to values Lower than the detection Limit <br /> (a) = Surrogate recoveries were outside acceptable ranges due to matrix effects. <br /> (b) = Surrogate recoveries were not calculated due to diLution of the sample below the detectable range for the surrogate. <br /> (c) = Matrix spike recoveries were outside acceptable ranges due to matrix effects. <br /> (d) = Relative Percent Difference (RPD) for duplicate analysis outside acceptance limits due to actual differences in <br /> }, the sample matrix. <br /> (e) = The Limit listed for flammability indicates the upper Limit for the test. Samples are not tested at temperatures <br /> above 140 Fahrenheit since only samples which will sustain ignition at temperatures below 140 are considered <br /> 9 � <br /> flammable. <br /> (f) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern. Results were quantified using a <br /> diesel standard, however, the hydrocarbon pattern did not match a diesel pattern_ <br /> i (g) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern. Results were quantified using a <br /> gasoline standard, however, the hydrocarbon pattern did not match a gasoline pattern. <br /> (h) = High dilution due to matrix effects <br /> QC SAMPLE IDENTIFICATIONS SUBCONTRACTED LABORATORY LOCATIONS <br /> MB = Method Blank SB = Storage Blank Core Laboratories: Aurora, Colorado *AU <br /> RB = Reagent Blank MS = Matrix Spike Casper, Wyoming *CA <br /> ICB = Initial Calibration Blank MSD = Matrix Spike Duplicate Corpus Christi, Texas *CC <br /> CCS = Continuing Calibration Blank MD = Matrix Duplicate Edison, New Jersey *ED <br /> CS = Calibration Standard SS = Blank Spike Houston, Texas (Env) *HE <br /> ICV = Initial Calibration SS = Surrogate Spike Houston, Texas (Pet) *HP <br /> Verification LCS = Laboratory Control Indianapolis, Indiana *IN <br /> CCV = Continuing Calibration Standard Lake Charles, Louisiana *tC <br /> Verification RS = Reference Standard Long Beach, California *L9 <br /> Valparaiso, Indiana *VP <br /> Bakersfield, California *BK <br /> i <br /> r 1250 Gene Autry Way Autry Way <br /> Anaheim, CA 92805 <br /> (714) 937-1094 /u/matt/Logs_n_forms/footer.form <br /> The aYuyura!yawns.oprnons«Irl ergetatpns cmta�•0'n ttas:QpaH Y.e�asW usqu mformalgn ar N1 maur:,i w{yn b,rip"'_t Ior wfpsg axdYarve 6M cpntdgnl y!Issg this re of n Gppn(rlade.TM analyt�.ai reruns.OPin'gns«inrBrPrYl2lmns <br /> _ eaPrassetl raprgap,l<M Oes!�,g—,al C«e 1-ahtx alwias.Co,Latfdal wre s,nowe gr,mases ro wa•r:n RY«rPPresmrration,eeprgrr or Impligrl,or enY IyPO,a•.tl expreuly niulaims aeux Y to t/q wotl ntay,prgfp•pparetrons w profit ab�eres5 01 <br /> aM dl,gas.coal«PlMr mineral.IXoperl Y.wsY w saM in tmnnecuon weh w h I«'w reason wnat5oever.tNa—'6naY ros be rewoOucetl,n wMle Pr e, <br /> Part,.n vnlllert YPProval PI CdB LdWratd�Ps. <br />